Abstract The recently reported19F‐detected dual‐optimized inverted1JCC1,n‐ADEQUATE experiment and the previously reported1H‐detected version have been modified to incorporateJ‐modulation, making it feasible to acquire all 1,1‐ and 1,n‐ADEQUATE correlations as well as1JCCandnJCChomonuclear scalar couplings in a single experiment. The experiments are demonstrated usingN,N‐dimethylamino‐2,5,6‐trifluoro‐3,4‐phthalonitrile andN,N‐dimethylamino‐3,4‐phthalonitrile.
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Use of Circular Statistics To Model αMan-(1→2)-αMan and αMan-(1→3)-α/βMan O -Glycosidic Linkage Conformation in 13 C-Labeled Disaccharides and High-Mannose Oligosaccharides
- Award ID(s):
- 1707660
- PAR ID:
- 10097485
- Date Published:
- Journal Name:
- Biochemistry
- Volume:
- 58
- Issue:
- 6
- ISSN:
- 0006-2960
- Page Range / eLocation ID:
- 546 to 560
- Format(s):
- Medium: X
- Sponsoring Org:
- National Science Foundation
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