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1. Constraining the timing and conditions of magmatism and metamorphism in the lower crust of the Southern California batholith using U-Pb zircon geochronology and Ti-in-zircon thermometry

   Robles, F.; Schwartz, J.; Miranda, E.; Klepeis, K.A.; and Mora-Klepeis, G. (October 2022, Geological Society of America Abstracts with Programs)

   The Southern California batholith contains a geologic record that can help clarify the timing of events that occurred during the Late Cretaceous (100-65 Ma) along the western margin of the North American Cordillera. The subduction of the oceanic conjugate Shatsky plateau beneath North America is postulated to have ended active magmatism in the arc at 88-70 Ma; however, the timing of this event is poorly constrained in Southern California. We use U-Pb laser ablation zircon petrochronology to document the timing and conditions of magmatism and metamorphism in the lower crust of the Cretaceous arc. We focus on the Cucamonga terrane in a part of the Southern California batholith located northeast of Los Angeles in the southeastern San Gabriel Mountains. These rocks contain exhumed lower crustal (7-9 kbar) rocks predominantly composed of granulite-facies metasedimentary rocks, migmatites, charnockite and dioritic to tonalitic gneiss. We report 20 new zircon dates from 11 samples, including 4 mafic biotite gneisses, 3 mylonitic tonalites, 2 charnockites, a quartzite, and a felsic pegmatite dike crosscutting granulite-facies metasedimentary rocks. New 206Pb/238U ages show that magmatism occurred in the Middle Jurassic (ca. 172-166 Ma), the Early Cretaceous (ca. 120-118 Ma), and the Late Cretaceous (88-86 Ma) at temperatures ranging from 740 to 800 oC. Granulite-facies metamorphism and partial melting of these rocks occurred during the 88-74 Ma interval at temperatures ranging from 730°C to 800oC. Our data indicate that high-temperature arc magmatism and granulite-facies metamorphism continued through the Late Cretaceous and overlapped in timing with postulated subduction of the conjugate Shatsky plateau from previous models. We speculate that termination of arc activity and cooling of the lower crust in response to plateau subduction must postdate ca. 74 Ma. 

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2. CONSTRAINING THE TIMING AND CONDITIONS OF MAGMATISM AND GRANULITE- TO UPPER AMPHIBOLITE-FACIES METAMORPHISM IN THE LOWER CRUST OF THE SOUTHERN CALIFORNIA BATHOLITH USING U-PB ZIRCON GEOCHRONOLOGY AND TI-IN-ZIRCON THERMOMETRY

   https://doi.org/10.1130/abs/2022AM-381996  

   Robles, Francine; Schwartz, Joshua; Miranda, Elena; Klepeis, Keith; Mora-Klepeis, Gabriela (January 2022, Geological Society of America abstracts)
3. CHICXULUB ZIRCON (AND APATITE!)

   Wittmann, Axel (May 2018, Annual meeting of the Meteoritical Society)

   Poster presentation of shock metamorphic features of accessory minerals in drill core samples of the Lower Peak Ring section of the Chicxulub impact crater. 

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4. Modeling apparent Pb loss in zircon U–Pb geochronology

   https://doi.org/10.5194/gchron-6-37-2024  

   Sharman, Glenn R.; Malkowski, Matthew A. (January 2024, Geochronology)

   Abstract. The loss of radiogenic Pb from zircon is known to be a major factor that can cause inaccuracy in the U–Pb geochronological system; hence, there is a need to better characterize the distribution of Pb loss in natural samples. Treatment of zircon by chemical abrasion (CA) has become standard practice in isotope dilution–thermal ionization mass spectrometry (ID-TIMS), but CA is much less commonly employed prior to in situ analysis via laser ablation–inductively coupled plasma–mass spectrometry (LA-ICP-MS) or secondary ionization mass spectrometry (SIMS). Differentiating the effects of low levels of Pb loss in Phanerozoic zircon with relatively low-precision in situ U–Pb dates, where the degree of Pb loss is insufficient to cause discernible discordance, is challenging. We show that U–Pb isotopic ratios that have been perturbed by Pb loss may be modeled by convolving a Gaussian distribution that represents random variations from the true isotopic value stemming from analytical uncertainty with a distribution that characterizes Pb loss. We apply this mathematical framework to model the distribution of apparent Pb loss in 10 igneous samples that have both non-CA LA-ICP-MS or SIMS U–Pb dates and an estimate of the crystallization age, either through CA U–Pb or 40Ar/39Ar geochronology. All but one sample showed negative age offsets that were unlikely to have been drawn from an unperturbed U–Pb date distribution. Modeling apparent Pb loss using the logit–normal distribution produced good fits with all 10 samples and showed two contrasting patterns in apparent Pb loss; samples where most zircon U–Pb dates undergo a bulk shift and samples where most zircon U–Pb dates exhibited a low age offset but fewer dates had more significant offset. Our modeling framework allows comparison of relative degrees of apparent Pb loss between samples of different age, with the first and second Wasserstein distances providing useful estimates of the total magnitude of apparent Pb loss. Given that the large majority of in situ U–Pb dates are acquired without the CA treatment, this study highlights a pressing need for improved characterization of apparent Pb-loss distributions in natural samples to aid in interpreting non-CA in situ U–Pb data and to guide future data collection strategies. 

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5. Nanoscale processes of trace element mobility in metamorphosed zircon

   https://doi.org/10.1007/s00410-019-1631-1  

   Peterman, E. M.; Reddy, S. M.; Saxey, D. W.; Fougerouse, D.; Snoeyenbos, D. R.; Rickard, W. D. (November 2019, Contributions to Mineralogy and Petrology)