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1. Benchmarking surface tension measurement method using two oscillation modes in levitated liquid metals

   https://doi.org/10.1038/s41526-021-00137-9  

   Brosius, Nevin; Ward, Kevin; Wilson, Evan; Karpinsky, Zachary; SanSoucie, Michael; Ishikawa, Takehiko; Matsumoto, Satoshi; Narayanan, Ranga (December 2021, npj Microgravity)

   null (Ed.)

   Abstract The Faraday forcing method in levitated liquid droplets has recently been introduced as a method for measuring surface tension using resonance. By subjecting an electrostatically levitated liquid metal droplet to a continuous, oscillatory, electric field, at a frequency nearing that of the droplet’s first principal mode of oscillation (known as mode 2), the method was previously shown to determine surface tension of materials that would be particularly difficult to process by other means, e.g., liquid metals and alloys. It also offers distinct advantages in future work involving high viscosity samples because of the continuous forcing approach. This work presents (1) a benchmarking experimental method to measure surface tension by excitation of the second principal mode of oscillation (known as mode 3) in a levitated liquid droplet and (2) a more rigorous quantification of droplet excitation using a projection method. Surface tension measurements compare favorably to literature values for Zirconium, Inconel 625, and Rhodium, using both modes 2 and 3. Thus, this new method serves as a credible, self-consistent benchmarking technique for the measurement of surface tension. 

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2. Demonstration of a container-less method for investigating high-temperature alloy properties using ED-XRD

   https://doi.org/10.1063/5.0213480  

   McKay, Frank; Bergeron, Kane; Roy, Amitava; Britt, S Thomas; SanSoucie, Michael P; Phillips, Brandon S; Raush, Jonathan; Sprunger, Phillip T (November 2024, Review of Scientific Instruments)

   As new alloys are being developed for additive manufacturing (AM) applications, questions related to the temperature-dependent structural and compositional stability of these alloys remain. In this work, the benefits and limitations of a unique method for testing this stability are presented. This system employs the use of polychromatic synchrotron light to perform energy-dispersive x-ray diffraction (ED-XRD) on an electrostatically levitated sample at high temperatures. In comparison with a traditional angular-dispersive setup, the container-less electrostatic levitation method has unique advantages, including quicker acquisition times, simultaneous compositional information through fluorescence emissions, a reduction in background noise, and, importantly, concurrent/subsequent measurement of thermophysical properties. This combined method is ideal for phase transition studies by holding the levitated sample at a stable position and temperature through controlled heating and temperature management. To illustrate these capabilities, we show ED-XRD data of the well-known martensitic phase transition (hcp to bcc) in Ti–6Al–4V. In addition, results from the novel alloy Ni51Cu44Cr5 are presented. This alloy is shown to maintain an fcc structure upon heating. However, the concentration of Cu is reduced at high temperatures, resulting in a decrease in the lattice constant. As concurrent thermophysical properties are probed, these preliminary structure and composition experiments demonstrate the capabilities of this technique to determine the composition–processing–structure–properties of metal alloys for AM. 

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3. Pattern formation in Faraday instability—experimental validation of theoretical models

   https://doi.org/10.1098/rsta.2022.0081  

   Dinesh, B.; Livesay, J.; Ignatius, I. B.; Narayanan, R. (April 2023, Philosophical Transactions of the Royal Society A: Mathematical, Physical and Engineering Sciences)

   n/a (Ed.)

   Two types of resonance-derived interfacial instability are reviewed with a focus on recent work detailing the effect of side walls on interfacial mode discretization. The first type of resonance is the mechanical Faraday instability, and the second is electrostatic Faraday instability. Both types of resonance are discussed for the case of single-frequency forcing. In the case of mechanical Faraday instability, inviscid theory can forecast the modal forms that one might expect when viscosity is taken into account. Experiments show very favourable validation with theory for both modal forms and onset conditions. Lowering of gravity is predicted to shift smaller wavelengths or choppier modes to lower frequencies. This is also validated by experiments. Electrostatic resonant instability is shown to lead to a pillaring mode that occurs at low wavenumbers, which is akin to Rayleigh Taylor instability. As in the case of mechanical resonance, experiments show favourable validation with theoretical predictions of patterns. A stark difference between the two forms of resonance is the observation of a gradual rise in the negative detuning instability in the case of mechanical Faraday and a very sharp one in the case of electrostatic resonance. This article is part of the theme issue ‘New trends in pattern formation and nonlinear dynamics of extended systems’. 

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4. Low-temperature Leidenfrost-like jumping of sessile droplets on microstructured surfaces

   https://doi.org/10.1038/s41567-024-02522-z  

   Huang, Wenge; Zhao, Lei; He, Xukun; Li, Yang; Collier, C Patrick; Zheng, Zheng; Liu, Jiansheng; Briggs, Dayrl P; Cheng, Jiangtao (May 2024, Nature Physics)

   Verberck, Bart (Ed.)

   The Leidenfrost effect—the levitation and hovering of liquid droplets on hot solid surfaces—generally requires a sufficiently high substrate temperature to activate liquid vaporization. Here we report the modulation of Leidenfrost-like jumping of sessile water microdroplets on micropillared surfaces at a relatively low temperature. Compared to traditional Leidenfrost effect occurring above 230 °C, the fin-array-like micropillars enable water microdroplets to levitate and jump off the surface within milliseconds at a temperature of 130 °C by triggering the inertia-controlled growth of individual vapour bubbles at the droplet base. We demonstrate that droplet jumping, resulting from momentum interactions between the expanding vapour bubble and the droplet, can be modulated by tailoring of the thermal boundary layer thickness through pillar height. This enables regulation of the bubble expansion between the inertia-controlled mode and the heat-transfer-limited mode. The two bubble-growth modes give rise to distinct droplet jumping behaviours characterized by constant velocity and constant energy regimes, respectively. This heating strategy allows the straightforward purging of wetting liquid droplets on rough or structured surfaces in a controlled manner, with potential applications including the rapid removal of fouling media, even when located in surface cavities. 

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5. Tilt Corrections for Normal Mode Observations on Ocean Bottom Seismic Data, an example from the PI-LAB experiment

   https://doi.org/10.26443/seismica.v1i1.196  

   Harmon, Nicholas; Laske, Gabi; Crawford, Wayne; Rychert, Catherine (October 2022, Seismica)

   Earth's normal modes are fundamental observations used in global seismic tomography to understand Earth structure. Land seismic station coverage is sufficient to constrain the broadest scale Earth structures. However, 70% of Earth's surface is covered by the oceans, hampering our ability to observe variations in local mode frequencies that contribute to imaging small-scale structures. Broadband ocean bottom seismometers can record spheroidal modes to fill in gaps in global data coverage. Ocean bottom recordings are contaminated by signals from complex interactions between ocean and solid Earth dynamics at normal mode frequencies. We present a method for correcting tilt on broadband ocean bottom seismometers by rotation. The correction improves the ability of some instruments to observe spheroidal modes down to 0S4. We demonstrate this method using 15 broadband ocean bottom seismometers from the PI-LAB array. We measure normal mode peak frequency shifts and compare with 1-D reference mode frequencies and predictions from 3-D global models. Our measurements agree with the 3-D models for modes between 0S14 - 0S37 with small but significant differences. These differences likely reflect real Earth structure. This suggests incorporating ocean bottom normal mode measurements into global inversions will improve models of global seismic velocity structure. 

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