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Creators/Authors contains: "Chmely, Stephen C."

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  1. ; ; ; (, Chemical Communications)
    Ball milling CaI 2 and [KN(SiMe 3 ) 2 ] in a 1 : 1 ratio without solvent, and then extracting the ground material with toluene, yields the synthetically valuable neutral amide [Ca(N(SiMe 3 ) 2 ) 2 ] in good yield, without the contamination by calciate species that complicates solution metathesis routes. The effects on yield of grinding time, milling frequency, and calcium halide identity are also examined. 
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