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Polymer matrix composites are popular in the aerospace industry due to their high strength to weight ratio. While they have become popular, understanding and predicting their specific damage evolution mechanisms remains a challenge especially in designing with damage tolerance criteria. One challenge often faced is the presence of surface damage either induced during manufacturing, machining, or service of a composite part. While many studies have investigated how quasi-static, low-velocity, and ballistic impact results in damage in the material, there remains a need to further understand the reduction in performance that results from such surface damage. In this work, micro-indentation was conducted on a unidirectional IM7/8552 laminate composite specimen to induce quasi-static impact damage that results in surface damage. The specimen was then loaded in tension to 33% of its expected failure load and imaged using synchrotron X-ray micro-computed tomography to qualitatively investigate the progression of surface damage into sub-surface damage. This work shows that at 33% of tensile failure load, surface damage propagates into delamination and fiber breakage of plies directly sub-surface. This work sheds light on the progression of surface damage at loads less than 50% of the ultimate strength of a unidirectional laminate composite. 

The dynamic information of lithium‐ion battery active materials obtained from coin cell‐based in‐situ characterizations might not represent the properties of the active material itself because many other factors in the cell could have impacts on the cell performance. To address this problem, a single particle cell was developed to perform the in‐situ characterization without the interference of inactive materials in the battery electrode as well as the X‐ray‐induced damage. In this study, the dynamic morphological and phase changes of selenium‐doped germanium (Ge_0.9Se_0.1) at the single particle level were investigated via synchrotron‐based in‐situ transmission X‐ray microscopy. The results demonstrate the good reversibility of Ge_0.9Se_0.1at high cycling rate that helps understand its good cycling performance and rate capability. This in‐situ and operando technique based on a single particle battery cell provides an approach to understanding the dynamic electrochemical processes of battery materials during charging and discharging at the particle level.