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Bishop, Camille; Thelen, Jacob L.; Gann, Eliot; Toney, Michael F.; Yu, Lian; DeLongchamp, Dean M.; Ediger, M. D. (, Proceedings of the National Academy of Sciences)We show that glasses with aligned smectic liquid crystal-like order can be produced by physical vapor deposition of a molecule without any equilibrium liquid crystal phases. Smectic-like order in vapor-deposited films was characterized by wide-angle X-ray scattering. A surface equilibration mechanism predicts the highly smectic-like vapor-deposited structure to be a result of significant vertical anchoring at the surface of the equilibrium liquid, and near-edge X-ray absorption fine structure (NEXAFS) spectroscopy orientation analysis confirms this prediction. Understanding of the mechanism enables informed engineering of different levels of smectic order in vapor-deposited glasses to suit various applications. The preparation of a glass with orientational and translational order from a nonliquid crystal opens up an exciting paradigm for accessing extreme anisotropy in glassy solids.more » « less
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Grundy, Lorena S.; Sethi, Gurmukh K.; Galluzzo, Michael D.; Loo, Whitney S.; Maslyn, Jacqueline A.; Teran, Alexander A.; Thelen, Jacob L.; Timachova, Ksenia; Reimer, Jeffrey A.; Madsen, Louis A.; et al (, ACS Macro Letters)
