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Organometallic Ni( ii ), Ni( iii ), and Ni( iv ) complexes relevant to carbon–carbon and carbon–oxygen bond formation reactions

https://doi.org/10.1039/D1QI01486B

Magallón, C. ; Griego, L. ; Hu, C. H. ; Company, A. ; Ribas, X. ; Mirica, L. M. ( March 2022 , Inorganic Chemistry Frontiers)

Herein, the pyridinophanetetradentate ligand 3,6,9-trimethyl-3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1(15),11,13-triene, PyNMe 3 , is used to isolate and structurally characterize well-defined organometallic Ni( ii ) and Ni( iii ) complexes bearing the cycloneophyl fragment, an alkyl/aryl C-donor ligand. Furthermore, spectroscopic and cryo-mass spectrometry studies suggest the formation of a transient Ni( iv ) organometallic complex, and its relevance to C–C and C–O bond formation reactivity studies is discussed.
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From symmetry to entropy: Crystal entropy difference strongly affects early stage phase transformation

https://doi.org/10.1063/1.5114974

Hu, C. H. ; Chen, Y. C. ; Yu, P. J. ; Fung, K. Y. ; Hsueh, Y. C. ; Liaw, P. K. ; Yeh, J. W. ; Hu, A. ( December 2019 , Applied Physics Letters)

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