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Intermolecular Hydrogen Bonding between Poly[( R )-3-hydroxybutyrate] (PHB) and Pseudoboehmite and Its Effect on Crystallization of PHB

https://doi.org/10.1021/acsapm.0c00758

Liu, Changhao; Jia, Meng; Qu, Jing; Noda, Isao; Chase, D. Bruce; Street, Reva; Rabolt, John F. (November 2020, ACS Applied Polymer Materials)
null (Ed.)
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Two-Dimensional Correlation Spectroscopy (2D-COS) Studies of Solution Mixtures in the Low Frequency Raman Region

https://doi.org/10.1177/0003702819848501

Xu, Shuyu; Bruce Chase, D.; Rabolt, John F.; Noda, Isao (May 2019, Applied Spectroscopy)

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Microstructure effects on the rheology of nanoclay‐filled PHB/LDPE blends

https://doi.org/10.1002/pc.25273

Karami, Samaneh; Nazockdast, Hossein; Ahmadi, Zahed; Rabolt, John F.; Noda, Isao; Chase, D. Bruce (February 2019, Polymer Composites)
null (Ed.)
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Crystallization Retardation of Ultrathin Films of Poly[(R)-3-hydroxybutyrate] and a Random Copolymer Poly[(R)-3-hydroxybutyrate-co-(R)-3-hydroxyhexanoate] on an Aluminum Oxide Surface,

https://doi.org/10.1021/acs.macromol.9b01214

Liu, Changhao; Noda, Isao; Chase, D. Bruce; Zhang, Yuying; Qu, Jing; Jia, Meng; Ni, Chaoying; Rabolt, John F. (January 2019, Macromolecules)
null (Ed.)
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Structure and Growth Habits of Solution-Grown Single Crystals of a Random Copolymer, Poly[(R)-3-hydroxybutyrate-co-(R)-3-hydroxyhexanoate]

Liu, Changhou; Noda, Isao; Martin, David; Chase, Bruce D.; Ni, Chao; Rabolt, John F. (October 2018, Polymer)

Single crystals of a random copolymer, Poly[(R)-3-hydroxybutyrate-co-(R)-3-hydroxyhexanoate] (PHBHx), with a relatively high (R)-3-hydroxyhexanoate (3HHx) content of 3.9 mol% were grown from dilute solutions over a wide range of crystallization temperatures (Tc) from -20 °C to 75 °C. Unlike Poly[(R)-3-hydroxybutyrate-co-(R)-3-hydroxyvalerate] (PHBV) which allows the 3-hydroxyvalerate (3HV) to be included into PHB lattice, 3HHx is excluded from the lattice as a non-crystallizable molecular defect. Remarkably, however, even at such a high defect content, all the samples (except for Tc = -20 °C) formed well-developed needle-shaped single crystals, with a crystal morphology similar to that found for crystals of the homopolymer PHB.
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