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Low-Valent Metal Ions as MOF Pillars: A New Route Toward Stable and Multifunctional MOFs

https://doi.org/10.1021/jacs.1c05564

Sikma, R. Eric ; Katyal, Naman ; Lee, Su-Kyung ; Fryer, Joseph W. ; Romero, Catherine G. ; Emslie, Samuel K. ; Taylor, Elinor L. ; Lynch, Vincent M. ; Chang, Jong-San ; Henkelman, Graeme ; et al ( September 2021 , Journal of the American Chemical Society)

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In situ formation and solid-state oxidation of a triselenane NSeN-pincer MOF

https://doi.org/10.1039/c9cc07851g

He, Shichao ; Allemond, Laynee L. ; Dunning, Samuel G. ; Reynolds, Joseph E. ; Lynch, Vincent M. ; Humphrey, Simon M. ( January 2020 , Chemical Communications)

Controlled partial decomposition of 2-selenonicotinic acid in the presence of Co 2+ or Ni 2+ resulted in the in situ formation of an unusual MOF based on triselenane ligands (RSeSeSeR) coordinated to M 2+ centers as NSeN-pincers. Post-synthetic oxidation by treatment with aqueous H 2 O 2 facilitates its solid-state conversion into a RSeO 2 − molecular coordination complex, which was tracked via powder X-ray diffraction studies and by single-crystal structural resolution of the final product.
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