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Award ID contains: 1953254

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  1. ; ; ; ; ; (, Acta Crystallographica Section E Crystallographic Communications)
    The crystal structure of the title sulfonamide, C 10 H 15 NO 2 S, comprises two molecules in the asymmetric unit. The S=O bond lengths of the sulfonamide functional group range from 1.428 (2) to 1.441 (2) Å, with S—C bond lengths of 1.766 (3) Å (for both molecules in the asymmetric unit), and S—N bond lengths of 1.618 (2) and 1.622 (3) Å, respectively. When both molecules are viewed down the N—S bond, the propyl group is gauche to the toluene moiety. In the crystal structure, molecules of the title compound are arranged in an intricate three-dimensional network that is formed via intermolecular C—H...O and N—H...O hydrogen bonds. The crystal structure was refined from a crystal twinned by inversion. 
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  2. ; ; ; ; ; ; (, Chemical Science)
    A room temperature stable Y(ii)bis(amide) has been prepared and fully characterized. The complex reacts withtert-butylisocyanide to make a rare example of a transition metal isocyanide, CN–Y(NHAr*)2. 
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  3. ; ; ; ; ; ; ; ; ; (, RSC Medicinal Chemistry)
    SAR on NRF2 inhibitor MSU38225 has led to a compound that inhibits expression of NRF2 target genes, reduces proliferation of lung cancer cells through G2/M arrest, and lowers cell migration. 
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  4. ; ; ; (, Dalton Transactions)
    Metal quinoline complexes were prepared using a quinoline-based proteasome inhibitor (Quin1) and an inactive quinoline ligand (Quin2), and their cytotoxicities are reported towards multiple myeloma-related cell lines. 
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  5. ; ; (, Organic & Biomolecular Chemistry)
    Treatment of isoxazoles with enamines leads to an inverse electron-demand hetero-Diels–Alder reaction that produces substituted pyridines in the presence of TiCl 4 (THF) 2 and titanium powder. The reaction is highly regioselective with only a single isomer of the product observed by GC/MS and tolerant of many common functional groups. The transformation was examined computationally, and it was found that TiCl 4 (or a similar Lewis acid) likely acts to catalyze the reaction. After the initial [4 + 2]-cycloaddition, the oxaza-[2.2.1]-bicycle produced likely ring opens before amine loss to give an N -oxide. The pyridine is then obtained after reduction with TiCl 4 and titanium powder. 
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  6. ; ; (, Results in Chemistry)
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  7. ; ; ; ; ; (, Molecular Cancer Therapeutics)
    null (Ed.)
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