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  1. ; ; (, Chemical communications)
    Direct photocatalytic C–H activation mediated by MoO2Cl2(bpy-tBu), a unique photoactive metal OXO, is presented. The limiting step, reoxidation to the Mo dioxo, is evaluated and proposed to occur via a key Cl− loss event. Photocatalyst degradation occurs upon substitution of bpy-tBu with H2O generated during catalysis. 
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