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   Dang, T. H. ; Hawecker, J. ; Rongione, E. ; Baez Flores, G. ; To, D. Q. ; Rojas-Sanchez, J. C. ; Nong, H. ; Mangeney, J. ; Tignon, J. ; Godel, F. ; et al ( December 2020 , Applied Physics Reviews)

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5. Strain‐Driven Mixed‐Phase Domain Architectures and Topological Transitions in Pb 1− x Sr x TiO 3 Thin Films

   https://doi.org/10.1002/adma.202203469  

   Kavle, Pravin ; Zorn, Jacob A. ; Dasgupta, Arvind ; Wang, Bo ; Ramesh, Maya ; Chen, Long‐Qing ; Martin, Lane W. ( August 2022 , Advanced Materials)

   The potential for creating hierarchical domain structures, or mixtures of energetically degenerate phases with distinct patterns that can be modified continually, in ferroelectric thin films offers a pathway to control their mesoscale structure beyond lattice‐mismatch strain with a substrate. Here, it is demonstrated that varying the strontium content provides deterministic strain‐driven control of hierarchical domain structures in Pb_1−xSr_xTiO₃ solid‐solution thin films wherein two types,c/aanda₁/a₂, of nanodomains can coexist. Combining phase‐field simulations, epitaxial thin‐film growth, detailed structural, domain, and physical‐property characterization, it is observed that the system undergoes a gradual transformation (with increasing strontium content) from droplet‐likea₁/a₂ domains in ac/adomain matrix, to a connected‐labyrinth geometry ofc/adomains, to a disconnected labyrinth structure of the same, and, finally, to droplet‐likec/adomains in ana₁/a₂ domain matrix. A relationship between the different mixed‐phase modulation patterns and its topological nature is established. Annealing the connected‐labyrinth structure leads to domain coarsening forming distinctive regions of parallelc/aanda₁/a₂ domain stripes, offering additional design flexibility. Finally, it is found that the connected‐labyrinth domain patterns exhibit the highest dielectric permittivity.

    

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