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1. Characterization of Additively Manufactured Metals from ADDERE Printing

   Foster, J. ; Kumpaty, S. ; Coen, L. ; Perkins, A. ; Gengler, M. ; Woida, S. ( November 2022 , ASME International Mechanical Engineering Congress and Exposition)

   IMECE2022-88299 Midwest Engineered Systems Inc. has created a novel laser wire metal deposition process, ADDere manufacturing. ADDere has a much higher deposition rate than powder bed fusion, making it ideal for large components. In this project, the mechanical properties of ADDere printed materials were tested and compared to typical values found in ASM publications to show the quality of materials manufactured by the ADDere printing process. A detailed material analysis was performed on samples made from Ti-6Al-4V and 17-4 PH stainless steel. This work builds upon an earlier study of samples made from 17-4 PH that were produced using a single direction pattern. In this project, the 17-4 PH samples were printed in a cross hatched pattern, and testing results were compared to existing data from single direction samples of the previous research. The Ti-6Al-4V samples were created in two builds. One using the uni-directional method and the other with the crossed pattern. Testing specimens were removed from the samples using a water jet cutter and further machined into ASTM tensile bars and metallurgic mounts to perform a thorough material evaluation. The Ti-6Al-4V sample met the expected values in the ASM literature, and the cross hatched 17-4 PH exhibited a higher hardness and better microstructure than the single direction samples from the previous work. It was also observed that when the Ti64 samples were manufactured in the cross hatched pattern, the properties indicated slight improvement and more homogeneity than those printed in single layer direction. The obtained results indicate that ADDere’s printing process can produce highly refined materials that are customizable with their expected uses. This work showcases an excellent industry collaboration of an undergraduate research experience. 

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2. Effect of Specimen Surface Area Size on Fatigue Strength of Additively Manufactured Ti-Al-4V Parts

   Pegues, Jonathan ; Roach, Michael ; Williamson, R. Scott ; Shamsaei, Nima ( August 2017 , 28th International Solid Freeform Fabrication Symposium - An Additive Manufacturing Conference)

   As additive manufacturing becomes an increasingly popular method for advanced manufacturing of components, there are many questions that need to be answered before these parts can be implemented for structural purposes. One of the most common concerns with additively manufactured parts is the reliability when subjected to cyclic loadings which has been shown to be highly sensitive to defects such as pores and lack of fusion between layers. It stands to reason that larger parts will inherently have more defects than smaller parts which may result in some sensitivity to surface area differences between these parts. In this research, Ti-6Al-4V specimens with various sizes were produced via a laser-based powder bed fusion method. Uniaxial fatigue tests based on ASTM standards were conducted to generate fatigue-life curves for comparison. Fractography on the fractured specimens was performed to distinguish failure mechanisms between specimen sets with different sizes. 

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3. Thermophysical Properties of Laser Powder Bed Fused Ti-6Al-4V and AlSi10Mg Alloys Made with Varying Laser Parameters

   https://doi.org/10.3390/ma16144920  

   Akwaboa, Stephen ; Zeng, Congyuan ; Amoafo-Yeboah, Nigel ; Ibekwe, Samuel ; Mensah, Patrick ( July 2023 , Materials)

   This study investigated the influence of diverse laser processing parameters on the thermophysical properties of Ti-6Al-4V and AlSi10Mg alloys manufactured via laser powder bed fusion. During fabrication, the laser power (50 W, 75 W, 100 W) and laser scanning speed (0.2 m/s, 0.4 m/s, 0.6 m/s) were adjusted while keeping other processing parameters constant. Besides laser processing parameters, this study also explored the impact of test temperatures on the thermophysical properties of the alloys. It was found that the thermophysical properties of L-PBF Ti-6Al-4V alloy samples were sensitive to laser processing parameters, while L-PBF AlSi10Mg alloy showed less sensitivity. In general, for the L-PBF Ti-6Al-4V alloy, as the laser power increased and laser scan speed decreased, both thermal diffusivity and conductivity increased. Both L-PBF Ti-6Al-4V and L-PBF AlSi10Mg alloys demonstrated similar dependence on test temperatures, with thermal diffusivity and conductivity increasing as the test temperature rose. The CALPHAD software Thermo-Calc (2023b), applied in Scheil Solidification Mode, was utilized to calculate the quantity of solution atoms, thus enhancing our understanding of observed thermal conductivity variations. A detailed analysis revealed how variations in laser processing parameters and test temperatures significantly influence the alloy’s resulting density, specific heat, thermal diffusivity, and thermal conductivity. This research not only highlights the importance of processing parameters but also enriches comprehension of the mechanisms influencing these effects in the domain of laser powder bed fusion.

    

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4. Synthesizing Ti–Ni Alloy Composite Coating on Ti–6Al–4V Surface from Laser Surface Modification

   https://doi.org/10.3390/met13020243  

   Chen, Yitao ; Newkirk, Joseph W. ; Liou, Frank ( February 2023 , Metals)

   In this work, a Ni-alloy Deloro-22 was laser-deposited on a Ti–6Al–4V bar substrate with multiple sets of laser processing parameters. The purpose was to apply laser surface modification to synthesize different combinations of ductile TiNi and hard Ti2Ni intermetallic phases on the surface of Ti–6Al–4V in order to obtain adjustable surface properties. Scanning electron microscopy, energy dispersion spectroscopy, and X-ray diffraction were applied to reveal the deposited surface microstructure and phase. The effect of processing parameters on the resultant compositions of TiNi and Ti2Ni was discussed. The hardness of the deposition was evaluated, and comparisons with the Ti–6Al–4V bulk part were carried out. They showed a significant improvement in surface hardness on Ti–6Al–4V alloys after laser processing, and the hardness could be flexibly adjusted by using this laser-assisted surface modification technique. 

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5. Contrasting the Role of Pores on the Stress State Dependent Fracture Behavior of Additively Manufactured Low and High Ductility Metals

   https://doi.org/10.3390/ma14133657  

   Wilson-Heid, Alexander E. ; Furton, Erik T. ; Beese, Allison M. ( July 2021 , Materials)

   This study investigates the disparate impact of internal pores on the fracture behavior of two metal alloys fabricated via laser powder bed fusion (L-PBF) additive manufacturing (AM)—316L stainless steel and Ti-6Al-4V. Data from mechanical tests over a range of stress states for dense samples and those with intentionally introduced penny-shaped pores of various diameters were used to contrast the combined impact of pore size and stress state on the fracture behavior of these two materials. The fracture data were used to calibrate and compare multiple fracture models (Mohr-Coulomb, Hosford-Coulomb, and maximum stress criteria), with results compared in equivalent stress (versus stress triaxiality and Lode angle) space, as well as in their conversions to equivalent strain space. For L-PBF 316L, the strain-based fracture models captured the stress state dependent failure behavior up to the largest pore size studied (2400 µm diameter, 16% cross-sectional area of gauge region), while for L-PBF Ti-6Al-4V, the stress-based fracture models better captured the change in failure behavior with pore size up to the largest pore size studied. This difference can be attributed to the relatively high ductility of 316L stainless steel, for which all samples underwent significant plastic deformation prior to failure, contrasted with the relatively low ductility of Ti-6Al-4V, for which, with increasing pore size, the displacement to failure was dominated by elastic deformation. 

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