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1. Twinning characteristics in rolled AZ31B magnesium alloy under three stress states

   https://doi.org/https://doi.org/10.1016/j.matchar.2021.111050  

   Carneiro, L. ; Culbertson, D. ; Zhu, X. ; Yu, Q. ; Jiang, Y. ( May 2021 , Materials characterization)

   Stress-strain responses and twinning characteristics are studied for a rolled AZ31B magnesium alloy under three different stress states: tension along the normal direction (NDT), compression along the rolled direction (RDC), and torsion about the normal direction (NDTOR) using companion specimens interrupted at incremental strain levels. Tension twinning is extensively induced in twinning-favorable NDT and RDC. All the six variants of tension twin are activated under NDT, whereas a maximum of four variants is activated under RDC. Under NDTOR, both tension twins and compression twins are activated at relatively large strains and twinning occurs in a small fraction of favored grainsmore »rather than in the majority of grains. Secondary and tertiary twins are observed in the favorably-orientated grains at high strain levels. Deformation under each stress state shows three stages of strain hardening rate: fast decrease (Stage I), sequential increase (Stage II), and progressive decrease (Stage III). The increase in the hardening rate, which is more significant under NDT and RDC as compared to NDTOR, is attributed to the hardening effect of twin boundaries and twinning texture-induced slip activities. The hardening effect of twin boundaries include the dynamic Hall-Petch hardening induced by the multiplication of twin boundaries (TBs) and twin-twin boundaries (TTBs) as well as the hardening effect associated with the energetically unfavorable TTB formation. When the applied plastic strain is larger than 0.05 under NDT and RDC, the tension twin volume fraction is higher than 50%. The twinning-induced texture leads to the activation of non-basal slips mainly in the twinned volume, i.e. prismatic slips under NDT and pyramidal slips under RDC. The low work hardening under NDTOR is due to the prevailing basal slips with reduced twinning activities under NDTOR.« less
2. Twinning in rolled AZ31B magnesium alloy under free-end torsion

   https://doi.org/https://doi.org/10.1016/j.msea.2020.140405  

   Carneiro, L. ; Culbertson, D. ; Yu, Q. ; Jiang, Y. ( January 2021 , Materials science engineering)

   The mechanical response and microstructure evolution in a rolled AZ31B magnesium alloy were experimentally characterized using companion thin-walled tubular specimens under free-end monotonic torsion. The tubular specimens were made with their axes along the normal direction of the rolled magnesium plate. The shear stress-shear strain response shows a subtle sigmodal shape that is composed of four distinctive stages of strain hardening. Basal slips and tension twinning are operated throughout the shear deformation. Both tension twinning and compressing twinning are favored. Growth and interaction of tension twins with multiple variants lead to formation of twin-twin boundaries (TTBs). The collective hardening effectsmore »by twin boundary (TB) and TTB result in a unique rise of the strain hardening rate in Stage II and III. In addition to primary twins, tension-compression double twins and tension-compression-tension tertiary twins with detectable sizes are observed in the tension-twin favorable grains whereas compression-tension double twins are detected in the tension-twin unfavorable grains; all of which become more observable with the increasing shear strain. During Stage IV deformation where TTB formation exhausts, non-basal prismatic slips become more significant and are responsible for the progressive decrease in strain hardening rate in this stage. Swift effect, which is commonly observed in textured materials, is evidenced under free-end torsion. The origin of Swift effect is confirmed to be dislocation slips at a shear strain less than 5% but is predominantly due to tension twinning at a larger plastic strain.« less
3. Effect of the State of Stress in the Fracturing and Micro-Seismic Activity of Hydraulically-Fractured Granite

   Gunarathna, G ; Goncalves da Silva, B ( January 2019 , US Rock Mechanics/Geomechanics Symposium)

   Hydraulic fracturing can be recognized as an emerging method used in the mining of heat in Enhanced Geothermal Systems as well as in the extraction of oil and gas entrapped within shale formations. While there are several experimental studies focusing on the initiation and propagation of hydraulically-induced fractures under uniaxial and biaxial loading conditions, a very limited number of experimental studies investigate the effect of triaxial loading conditions on fracture initiation and propagation. This study describes an experimental setup, which was designed to allow one to independently apply and control three orthogonal stresses in prismatic granite specimens while simultaneously applyingmore »a hydraulic pressure inside pre-fabricated flaws. Moreover, the test setup allows one to observe and subsequently interpret the fracturing processes through visual and acoustic emission (AE) monitoring. The observations obtained in the current study using a triaxial state of stress were interpreted and compared with existing experimental studies that used other states of stress. It was observed that whitening of some grains and high-amplitude AE events occurred where visible cracks eventually developed for the triaxial state of stress investigated. Comparison with previous studies, in which only vertical loads (uniaxial) were applied, shows that the aperture of the hydraulically-induced fractures for the triaxial condition is significantly smaller than for the uniaxial loadings and that the coalescence patterns are, in general, stress-state-dependent. In terms of AE data, the total number of AE events in the specimens subject to triaxial stresses were significantly higher than in the tests using uniaxial stresses, even though most of the events (65%) had a relatively low-amplitude (<50dB) in contrast to the uniaxial tests, in which low-amplitude events were typically less than 50%.« less
4. Traveling surface undulation on a Ni-Mn-Ga single crystal elemen

   Armstrong, Andrew ; Karki, Bibek ; Smith, Aaron ; Müllner, Peter ( June 2021 , Smart materials and structures)

   Active materials couple a stimulus (electrical, magnetic, thermal) with a mechanical response. Typical materials such as piezoelectrics strain as bulk materials to the stimuli. Here we consider an undulation created by heterogeneous deformation within a magnetic shape memory alloy (MSM) transducer. We study the mechanical response of an MSM element vs. two surface treatments: a polished state with minimal surface stresses, and a micropeened state with compressive surface stress. The polished element had a sharp-featured, faceted trough shape. The micropeened element had a smooth trough shape and an additional crest. The undulation was created by a rotating localized magnetic field,more »which caused heterogeneous variation of the twin-microstructure. For the polished and micropeened elements, the twin-microstructures were coarse and fine, respectively. For the polished element, the undulation moved by the nucleation of a few twin boundaries, which traveled along the entire element. For the micropeened sample, the twin boundaries moved back and forth over a short distance, thereby creating a dense twin lamellar, which formed the trough. The motion of the lamellar approximated the single thick twin while allowing additional degrees of freedom due to increased mobile interface density and different initial conditions of domain volume fraction. The dense twin microstructure also smoothed the magnetic flux pattern. The undulation amplitude was about 40 μm for the sample in both treatments.« less
5. Quantifying microscale drivers for fatigue failure via coupled synchrotron X-ray characterization and simulations

   https://doi.org/10.1038/s41467-020-16894-2  

   Gustafson, Sven ; Ludwig, Wolfgang ; Shade, Paul ; Naragani, Diwakar ; Pagan, Darren ; Cook, Phil ; Yildirim, Can ; Detlefs, Carsten ; Sangid, Michael D. ( June 2020 , Nature Communications)

   During cyclic loading, localization of intragranular deformation due to crystallographic slip acts as a precursor for crack initiation, often at coherent twin boundaries. A suite of high-resolution synchrotron X-ray characterizations, coupled with a crystal plasticity simulation, was conducted on a polycrystalline nickel-based superalloy microstructure near a parent-twin boundary in order to understand the deformation localization behavior of this critical, 3D microstructural configuration. Dark-field X-ray microscopy was spatially linked to high energy X-ray diffraction microscopy and X-ray diffraction contrast tomography in order to quantify, with cutting-edge resolution, an intragranular misorientation and high elastic strain gradients near a twin boundary. Thesemore »observations quantify the extreme sub-grain scale stress gradients present in polycrystalline microstructures, which often lead to fatigue failure.

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