skip to main content


Title: Morphological and microstructural investigation of the non-planar interface formed in solid-state metal additive manufacturing by additive friction stir deposition
Additive friction stir deposition (AFSD) is an emerging solid-state metal additive manufacturing technology renowned for strong interface adhesion and isotropic mechanical properties. This is postulated to result from the material flow phenomena near the interface, but experimental corroboration has remained absent. Here, we seek to understand the interface formed in AFSD via morphological and microstructural investigation, wherein the non-planar interfacial morphology is characterized on the track-scale (centimeter scale) using X-ray computed tomography and the material deformation history is explored by microstructure mapping at the interfacial regions. X-ray computed tomography reveals unique 3D features at the interface with significant macroscopic material mixing. In the out-of-plane direction, the deposited material inserts below the initial substrate surface in the feed-rod zone, while the substrate surface surges upwards in the tool protrusion-affected zone. Complex 3D structures like fins and serrations form on the advancing side, leading to structural interlocking; on the retreating side, the interface manifests as a smooth sloped surface. Microstructure mapping reveals a uniform thermomechanical history for the deposited material, which develops a homogeneous, almost fully recrystallized microstructure. The substrate surface develops partially recrystallized microstructures that are location-dependent; more intra-granular orientation gradients are found in the regions further away from the centerline of the deposition track. From these observations, we discuss the mechanisms for interfacial material flow and interface morphology formation during AFSD.  more » « less
Award ID(s):
1853893
NSF-PAR ID:
10222574
Author(s) / Creator(s):
; ; ; ;
Date Published:
Journal Name:
Additive manufacturing
Volume:
35
ISSN:
2214-7810
Page Range / eLocation ID:
101293
Format(s):
Medium: X
Sponsoring Org:
National Science Foundation
More Like this
  1. null (Ed.)
    Abstract Aerosol jet printing (AJP) is a direct-write additive manufacturing technique, which has emerged as a high-resolution method for the fabrication of a broad spectrum of electronic devices. Despite the advantages and critical applications of AJP in the printed-electronics industry, AJP process is intrinsically unstable, complex, and prone to unexpected gradual drifts, which adversely affect the morphology and consequently the functional performance of a printed electronic device. Therefore, in situ process monitoring and control in AJP is an inevitable need. In this respect, in addition to experimental characterization of the AJP process, physical models would be required to explain the underlying aerodynamic phenomena in AJP. The goal of this research work is to establish a physics-based computational platform for prediction of aerosol flow regimes and ultimately, physics-driven control of the AJP process. In pursuit of this goal, the objective is to forward a three-dimensional (3D) compressible, turbulent, multiphase computational fluid dynamics (CFD) model to investigate the aerodynamics behind: (i) aerosol generation, (ii) aerosol transport, and (iii) aerosol deposition on a moving free surface in the AJP process. The complex geometries of the deposition head as well as the pneumatic atomizer were modeled in the ansys-fluent environment, based on patented designs in addition to accurate measurements, obtained from 3D X-ray micro-computed tomography (μ-CT) imaging. The entire volume of the constructed geometries was subsequently meshed using a mixture of smooth and soft quadrilateral elements, with consideration of layers of inflation to obtain an accurate solution near the walls. A combined approach, based on the density-based and pressure-based Navier–Stokes formation, was adopted to obtain steady-state solutions and to bring the conservation imbalances below a specified linearization tolerance (i.e., 10−6). Turbulence was modeled using the realizable k-ε viscous model with scalable wall functions. A coupled two-phase flow model was, in addition, set up to track a large number of injected particles. The boundary conditions of the CFD model were defined based on experimental sensor data, recorded from the AJP control system. The accuracy of the model was validated using a factorial experiment, composed of AJ-deposition of a silver nanoparticle ink on a polyimide substrate. The outcomes of this study pave the way for the implementation of physics-driven in situ monitoring and control of AJP. 
    more » « less
  2. M. Wiercigroch, editof-in-chief (Ed.)
    Additive manufacturing (AM) is known to generate large magnitudes of residual stresses (RS) within builds due to steep and localized thermal gradients. In the current state of commercial AM technology, manufacturers generally perform heat treatments in effort to reduce the generated RS and its detrimental effects on part distortion and in-service failure. Computational models that effectively simulate the deposition process can provide valuable insights to improve RS distributions. Accordingly, it is common to employ Computational fluid dynamics (CFD) models or finite element (FE) models. While CFD can predict geometric and thermal fluid behavior, it cannot predict the structural response (e.g., stress–strain) behavior. On the other hand, an FE model can predict mechanical behavior, but it lacks the ability to predict geometric and fluid behavior. Thus, an effectively integrated thermofluidic–thermomechanical modeling framework that exploits the benefits of both techniques while avoiding their respective limitations can offer valuable predictive capability for AM processes. In contrast to previously published efforts, the work herein describes a one-way coupled CFDFEA framework that abandons major simplifying assumptions, such as geometric steady-state conditions, the absence of material plasticity, and the lack of detailed RS evolution/accumulation during deposition, as well as insufficient validation of results. The presented framework is demonstrated for a directed energy deposition (DED) process, and experiments are performed to validate the predicted geometry and RS profile. Both single- and double-layer stainless steel 316L builds are considered. Geometric data is acquired via 3D optical surface scans and X-ray micro-computed tomography, and residual stress is measured using neutron diffraction (ND). Comparisons between the simulations and measurements reveal that the described CFD-FEA framework is effective in capturing the coupled thermomechanical and thermofluidic behaviors of the DED process. The methodology presented is extensible to other metal AM processes, including power bed fusion and wire-feed-based AM. 
    more » « less
  3. Andrew Yeh-Ching Nee, editor-ion-chief (Ed.)
    Wire arc additive manufacturing (WAAM) has received increasing use in 3D printing because of its high deposition rates suitable for components with large and complex geometries. However, the lower forming accuracy of WAAM than other metal additive manufacturing methods has imposed limitations on manufacturing components with high precision. To resolve this issue, we herein implemented the hybrid manufacturing (HM) technique, which integrated WAAM and subtractive manufacturing (via a milling process), to attain high forming accuracy while taking advantage of both WAAM and the milling process. We describe in this paper the design of a robot-based HM platform in which the WAAM and CNC milling are integrated using two robotic arms: one for WAAM and the other for milling immediately following WAAM. The HM was demonstrated with a thin-walled aluminum 5356 component, which was inspected by X-ray micro-computed tomography (μCT) for porosity visualization. The temperature and cutting forces in the component under milling were acquired for analysis. The surface roughness of the aluminum component was measured to assess the surface quality. In addition, tensile specimens were cut from the components using wire electrical discharge machining (WEDM) for mechanical testing. Both machining quality and mechanical properties were found satisfactory; thus the robot-based HM platform was shown to be suitable for manufacturing high-quality aluminum parts. 
    more » « less
  4. The objective of this paper is to experimentally validate the graph-based approach that was advanced in our previous work for predicting the heat flux in metal additive manufactured parts. We realize this objective in the specific context of the directed energy deposition (DED) additive manufacturing process. Accordingly, titanium alloy (Ti6Al4V) test parts (cubes) measuring 12.7 mm × 12.7 mm × 12.7 mm were deposited using an Optomec hybrid DED system at the University of Nebraska-Lincoln (UNL). A total of six test parts were manufactured under varying process settings of laser power, material flow rate, layer thickness, scan velocity, and dwell time between layers. During the build, the temperature profiles for these test parts were acquired using a single thermocouple affixed to the substrate (also Ti6Al4V). The graph-based approach was tailored to mimic the experimental DED process conditions. The results indicate that the temperature trends predicted from the graph theoretic approach closely match the experimental data; the mean absolute percentage error between the experimental and predicted temperature trends were in the range of 6% ∼ 15%. This work thus lays the foundation for predicting distortion and the microstructure evolved in metal additive manufactured parts as a function of the heat flux. In our forthcoming research we will focus on validating the model in the context of the laser powder bed fusion process.

     
    more » « less
  5. The continued development of metal additive manufacturing (AM) has expanded the engineering metallic alloys for which these processes may be applied, including beta-titanium alloys with desirable strength-to-density ratios. To understand the response of beta-titanium alloys to AM processing, solidification and microstructure evolution needs to be investigated. In particular, thermal gradients (Gs) and solidification velocities (Vs) experienced during AM are needed to link processing to microstructure development, including the columnar-to-equiaxed transition (CET). In this work, in situ synchrotron X-ray radiography of the beta-titanium alloy Ti-10V-2Fe-3Al (wt.%) (Ti-1023) during simulated laser-powder bed fusion (L-PBF) was performed at the Advanced Photon Source at Argonne National Laboratory, allowing for direct determination of Vs. Two different computational modeling tools, SYSWELD and FLOW-3D, were utilized to investigate the solidification conditions of spot and raster melt scenarios. The predicted Vs obtained from both pieces of computational software exhibited good agreement with those obtained from in situ synchrotron X-ray radiography measurements. The model that accounted for fluid flow also showed the ability to predict trends unobservable in the in situ synchrotron X-ray radiography, but are known to occur during rapid solidification. A CET model for Ti-1023 was also developed using the Kurz–Giovanola–Trivedi model, which allowed modeled Gs and Vs to be compared in the context of predicted grain morphologies. Both pieces of software were in agreement for morphology predictions of spot-melts, but drastically differed for raster predictions. The discrepancy is attributable to the difference in accounting for fluid flow, resulting in magnitude-different values of Gs for similar Vs. 
    more » « less