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Title: Communication—Design of Heated Cells for In Situ Absorption and Reflectance UV–Vis Spectroelectrochemistry
Spectroelectrochemistry (SEC) enables in-operando UV–vis study of electrochemical cells to explore the evolution of different cell components and understand cell mechanisms. Researchers have demonstrated various custom UV–vis cell designs to accommodate SEC experiments. However, existing designs do not easily permit temperature ramp techniques to examine the effects of rapidly changing cell temperature or high temperature conditions on cell mechanisms. This communication presents two easy-to-replicate, low-cost cell designs that are incorporable with existing UV–vis systems (transmittance, reflectance) and enable high temperature, rapid heating SEC experiments. Each cell design was tested to evaluate temperature ramp and sealing performance.  more » « less
Award ID(s):
1936636
PAR ID:
10353870
Author(s) / Creator(s):
; ; ; ; ; ; ; ;
Date Published:
Journal Name:
Journal of The Electrochemical Society
Volume:
169
Issue:
6
ISSN:
0013-4651
Page Range / eLocation ID:
066502
Format(s):
Medium: X
Sponsoring Org:
National Science Foundation
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