skip to main content


Title: Test of the Effective Stress Law for Semibrittle Deformation Using Isostatic and Triaxial Load Paths
Abstract

For brittle friction and rock deformation, the coefficientαin the general effective stress relationσe = σ − αPpcan be approximated as unity with sufficient accuracy. However, it is uncertain ifαdeviates from unity for semibrittle flow when both brittle and intracrystalline‐plastic deformation is involved. We conducted triaxial and isostatic compression experiments on synthetic salt‐rocks (∼300 ppm water) at room temperature to test the effective stress relation in the semibrittle regime using silicone oil and argon gas as pore fluids. Confining and pore pressures were cycled while their difference (differential pressure) was kept constant, such that changes in the mechanical behavior would indicate deviation ofαfrom unity. Microstructural observations were used to determine the dependence ofαon true area of grain contact from asperity yielding. In triaxial compression experiments, semibrittle flow involves grain boundary cracking and sliding, and intragranular dislocation glide and cracking. Flow strength remains constant for changes in pore fluid pressure of more than two orders of magnitude. In isostatic compression experiments, samples show combined processes of microcracking, grain boundary sliding, dislocation glide, and fluid‐assisted grain boundary migration recrystallization. Volumetric strain depends directly on the differential pressures (i.e.,αequals one). Analysis of grain‐contact area in both experiments indicates thatαis independent of the true area of contact defined by plastic yielding at grain boundaries. The observation ofαeffectively equals one may be explained by operation of pressure‐independent intracrystalline‐plastic mechanisms and transmission of pore pressure at grain boundaries through thin fluid films.

 
more » « less
Award ID(s):
1361996
NSF-PAR ID:
10361457
Author(s) / Creator(s):
 ;  ;  
Publisher / Repository:
DOI PREFIX: 10.1029
Date Published:
Journal Name:
Journal of Geophysical Research: Solid Earth
Volume:
126
Issue:
5
ISSN:
2169-9313
Format(s):
Medium: X
Sponsoring Org:
National Science Foundation
More Like this
  1. Abstract

    The operation of fracture, diffusion, and intracrystalline‐plastic micromechanisms during semibrittle deformation of rock is directly relevant to understanding mechanical behavior across the brittle‐plastic transition in the crust. An outstanding question is whether (1) the micromechanisms of semibrittle flow can be considered to operate independently, as represented in typical crustal strength profiles across the brittle to plastic transition, or (2) the micromechanisms are coupled such that the transition is represented by a distinct rheology with dependency on effective pressure, temperature, and strain rate. We employ triaxial stress‐cycling experiments to investigate elastic‐plastic and viscoelastic behaviors during semibrittle flow in two distinctly different monomineralic, polycrystalline, synthetic salt‐rocks. During semibrittle flow at high differential stress, granular, low‐porosity, work‐hardened salt‐rocks deform predominantly by grain‐boundary sliding and wing‐crack opening accompanied by minor intragranular dislocation glide. In contrast, fully annealed, near‐zero porosity salt‐rocks flow at lower differential stress by intragranular dislocation glide accompanied by grain‐boundary sliding and opening. Grain‐boundary sliding is frictional during semibrittle flow at higher strain rates, but the associated dispersal of water from fluid inclusions along boundaries can activate fluid‐assisted diffusional sliding at lower strain rates. Changes in elastic properties with semibrittle flow largely reflect activation of sliding along closed grain boundaries. Observed microstructures, pronounced hysteresis and anelasticity during cyclic stressing after semibrittle flow, and stress relaxation behaviors indicate coupled operation of micromechanisms leading to a distinct rheology (hypothesis 2 above).

     
    more » « less
  2. Abstract

    Large earthquakes and slow slip events typically nucleate along plate boundaries near the depth limit of the seismogenic zone, which is also recognized as the brittle‐plastic transition zone (BPT). HighVp/Vsratios are commonly observed at the BPT in subduction zones, indicating the presence of aqueous fluid in pore spaces. We conducted experiments to investigate the rheology of quartz with different fluid fractions at deformation conditions that cross the BPT. The strengths of quartz aggregates with fluid‐filled porosities of 5–25 vol% are significantly lower than predicted by wet quartzite flow laws, and decrease with increasing fluid fraction. Recovered samples deformed in the ductile regime exhibit S‐C´ mylonitic structures characterized by elongate grains, shear localization and fluid segregation. Variations in strength are explained by a combination of a constitutive law for dislocation creep that includes the geometric effects of fluid fraction, a friction law that includes the effect of fluid fraction through its role on the real area of contact, and an empirical function to describe the smooth brittle‐plastic transition. Our results indicate that the presence of fluid‐filled porosity promotes significant weakening in shear zones, and that variations in fluid fraction (together with temperature) can explain transitions in the spectrum of slip behaviors observed along plate boundaries.

     
    more » « less
  3. Abstract

    Critical processes including seismic faulting, reservoir compartmentalization, and borehole failure involve high‐pressure mechanical behavior and strain localization of sedimentary rocks such as sandstone. Sand is often used as a model material to study the mechanical behavior of poorly lithified sandstone. Recent studies exploring the multi‐scale mechanics of sand have characterized the brittle, low‐pressure regime of behavior; however, limited work has provided insights into the ductile, high‐pressure regime of behavior viain‐situmeasurements. Critical features of the ductile regime, including grain breakage, grain micromechanics, and volumetric strain behavior therefore remain under‐explored. Here, we use a new high‐pressure triaxial apparatus within‐situx‐ray tomography to provide new insights into deformation banding, grain breakage, and grain micromechanics in Ottawa sand subjected to triaxial compression under confining pressures between 10 and 45 MPa. We observed strain‐hardening at pressures above 15 MPa and strain‐neutral responses at pressures below 15 MPa. Compacting shear bands and grain breakage were observed at all pressures with no significant variation due to grain size, except for minor increases in breakage in less‐rounded sands. Grain breakage emerged at stress levels lower than the assumed yield threshold and more intense breakage was associated with thinner deformation bands. Contact sliding at inter‐grain contacts demonstrated a bifurcation into a bimodal distribution, with intense sliding within deformation bands and reduced but non‐negligible sliding outside of deformation bands, suggesting that off‐band zones remain mechanically active during strain hardening.

     
    more » « less
  4. The strength of lithospheric plates is a central component of plate tectonics, governed by brittle processes in the shallow portion of the plate and ductile behavior in the deeper portion. We review experimental constraints on ductile deformation of olivine, the main mineral in the upper mantle and thus the lithosphere. Olivine deforms by four major mechanisms: low-temperature plasticity, dislocation creep, dislocation-accommodated grain-boundary sliding (GBS), and diffusion-accommodated grain-boundary sliding (diffusion creep). Deformation in most of the lithosphere is dominated by GBS, except in shear zones—in which diffusion creep dominates—and in the brittle-ductile transition—in which low-temperature plasticity may dominate. We find that observations from naturally deformed rocks are consistent with extrapolation of the experimentally constrained olivine flow laws to geological conditions but that geophysical observations predict a weaker lithosphere. The causes of this discrepancy are unresolved but likely reside in the uncertainty surrounding processes in the brittle-ductile transition, at which the lithosphere is strongest. ▪ Ductile deformation of the lithospheric mantle is constrained by experimental data for olivine. ▪ Olivine deforms by four major mechanisms: low-temperature plasticity, dislocation creep, dislocation-accommodated grain-boundary sliding, and diffusion creep. ▪ Observations of naturally deformed rocks are consistent with extrapolation of olivine flow laws from experimental conditions. ▪ Experiments predict stronger lithosphere than geophysical observations, likely due to gaps in constraints on deformation in the brittle-ductile transition. 
    more » « less
  5. Abstract Carbonate sediments play a prominent role on the global geological stage as they store more than $$60\%$$ 60 % of world’s oil and $$40\%$$ 40 % of world’s gas reserves. Prediction of the deformation and failure of porous carbonates is, therefore, essential to minimise reservoir compaction, fault reactivation, or wellbore instability. This relies on our understanding of the mechanisms underlying the observed inelastic response to fluid injection or deviatoric stress perturbations. Understanding the impact of deformation/failure on the hydraulic properties of the rock is also essential as injection/production rates will be affected. In this work, we present new experimental results from triaxial deformation experiments carried out to elucidate the behaviour of a porous limestone reservoir analogue (Savonnières limestone). Drained triaxial and isotropic compression tests were conducted at five different confining pressures in dry and water-saturated conditions. Stress–strain data and X-ray tomography images of the rock indicate two distinct types of deformation and failure regimes: at low confinement (10 MPa) brittle failure in the form of dilatant shear banding was dominant; whereas at higher confinement compaction bands orthogonal to the maximum principal stress formed. In addition to the pore pressure effect, the presence of water in the pore space significantly weakened the rock, thereby shrinking the yield envelope compared to the dry conditions, and shifted the brittle–ductile transition to lower effective confining pressures (from 35 MPa to 29 MPa). Finally, permeability measurements during deformation show a reduction of an order of magnitude in the ductile regime due to the formation of the compaction bands. These results highlight the importance of considering the role of the saturating fluid in the brittle–ductile response of porous rocks and elucidate some of the microstructural processes taking place during this transition. 
    more » « less