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1. Production and validation of scintillating structural components from low-background Poly(ethylene naphthalate)

   https://doi.org/10.1088/1748-0221/17/01/P01010  

   Efremenko, Y. ; Febbraro, M. ; Fischer, F. ; Guitart Corominas, M. ; Gusev, K. ; Hackett, B. ; Hayward, C. ; Hodák, R. ; Krause, P. ; Majorovits, B. ; et al ( January 2022 , Journal of Instrumentation)

   Abstract Poly Ethylene Naphthalate (PEN) is an industrial polymer plastic which is investigated as a low background, transparent, scintillating and wavelength shifting structural material. PEN scintillates in the blue region and has excellent mechanical properties both at room and cryogenic temperatures. Thus, it is an ideal candidate for active structural components in experiments for the search of rare events like neutrinoless double-beta decay or dark matter recoils. Such optically active structures improve the identification and rejection efficiency of backgrounds events, like this improving the sensitivity of experiments. This paper reports on the production of radiopure and transparent PEN plates These structures can be used to mount germanium detectors operating in cryogenic liquids (LAr, LN). Thus, as first application PEN holders will be used to mount the Ge detectors in the Legend -200 experiment. The whole process from cleaning the raw material to testing the PEN active components under final operational conditions is reported. 

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2. R &D of wavelength-shifting reflectors and characterization of the quantum efficiency of tetraphenyl butadiene and polyethylene naphthalate in liquid argon

   https://doi.org/10.1140/epjc/s10052-022-10383-0  

   Araujo, G. R. ; Baudis, L. ; McFadden, N. ; Krause, P. ; Schönert, S. ; Wu, V. H. ( May 2022 , The European Physical Journal C)

   Abstract Detectors based on liquid argon (LAr) often require surfaces that can shift vacuum ultraviolet (VUV) light and reflect the visible shifted light. For the LAr instrumentation of the LEGEND-200 neutrinoless double beta decay experiment, several square meters of wavelength-shifting reflectors (WLSR) were prepared: the reflector Tetratex® (TTX) was in-situ evaporated with the wavelength shifter tetraphenyl butadiene (TPB). For even larger detectors, TPB evaporation will be more challenging and plastic films of polyethylene naphthalate (PEN) are considered as an option to ease scalability. In this work, we first characterized the absorption (and reflectivity) of PEN, TPB (and TTX) films in response to visible light. We then measured TPB and PEN coupled to TTX in a LAr setup equipped with a VUV sensitive photomultiplier tube. The effective VUV photon yield in the setup was first measured using an absorbing reference sample, and the VUV reflectivity of TTX quantified. The characterization and simulation of the setup along with the measurements and modelling of the optical parameters of TPB, PEN and TTX allowed to estimate the absolute quantum efficiency (QE) of TPB and PEN in LAr (at 87K) for the first time: these were found to be above 67 and 49%, respectively (at 90% CL). These results provide relevant input for the optical simulations of experiments that use TPB in LAr, such as LEGEND-200, and for experiments that plan to use TPB or PEN to shift VUV scintillation light. 

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3. $$\alpha $$-event characterization and rejection in point-contact HPGe detectors

   https://doi.org/10.1140/epjc/s10052-022-10161-y  

   Arnquist, I. J. ; Avignone, F. T. ; Barabash, A. S. ; Barton, C. J. ; Bertrand, F. E. ; Blalock, E. ; Bos, B. ; Busch, M. ; Buuck, M. ; Caldwell, T. S. ; et al ( March 2022 , The European Physical Journal C)

   Abstract P-type point contact (PPC) HPGe detectors are a leading technology for rare event searches due to their excellent energy resolution, low thresholds, and multi-site event rejection capabilities. We have characterized a PPC detector’s response to $$\alpha $$ α particles incident on the sensitive passivated and p $$^+$$ + surfaces, a previously poorly-understood source of background. The detector studied is identical to those in the Majorana Demonstrator experiment, a search for neutrinoless double-beta decay ( $$0\nu \beta \beta $$ 0 ν β β ) in $$^{76}$$ 76 Ge. $$\alpha $$ α decays on most of the passivated surface exhibit significant energy loss due to charge trapping, with waveforms exhibiting a delayed charge recovery (DCR) signature caused by the slow collection of a fraction of the trapped charge. The DCR is found to be complementary to existing methods of $$\alpha $$ α identification, reliably identifying $$\alpha $$ α background events on the passivated surface of the detector. We demonstrate effective rejection of all surface $$\alpha $$ α events (to within statistical uncertainty) with a loss of only 0.2% of bulk events by combining the DCR discriminator with previously-used methods. The DCR discriminator has been used to reduce the background rate in the $$0\nu \beta \beta $$ 0 ν β β region of interest window by an order of magnitude in the Majorana Demonstrator   and will be used in the upcoming LEGEND-200 experiment. 

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4. Electrode and electrolyte configurations for low frequency motion energy harvesting based on reverse electrowetting

   https://doi.org/10.1038/s41598-021-84414-3  

   Adhikari, Pashupati R. ; Tasneem, Nishat T. ; Reid, Russell C. ; Mahbub, Ifana ( March 2021 , Scientific Reports)

   Increasing demand for self-powered wearable sensors has spurred an urgent need to develop energy harvesting systems that can reliably and sufficiently power these devices. Within the last decade, reverse electrowetting-on-dielectric (REWOD)-based mechanical motion energy harvesting has been developed, where an electrolyte is modulated (repeatedly squeezed) between two dissimilar electrodes under an externally applied mechanical force to generate an AC current. In this work, we explored various combinations of electrolyte concentrations, dielectrics, and dielectric thicknesses to generate maximum output power employing REWOD energy harvester. With the objective of implementing a fully self-powered wearable sensor, a “zero applied-bias-voltage” approach was adopted. Three different concentrations of sodium chloride aqueous solutions (NaCl-0.1 M, NaCl-0.5 M, and NaCl-1.0 M) were used as electrolytes. Likewise, electrodes were fabricated with three different dielectric thicknesses (100 nm, 150 nm, and 200 nm) of Al₂O₃and SiO₂with an additional layer of CYTOP for surface hydrophobicity. The REWOD energy harvester and its electrode–electrolyte layers were modeled using lumped components that include a resistor, a capacitor, and a current source representing the harvester. Without using any external bias voltage, AC current generation with a power density of 53.3 nW/cm²was demonstrated at an external excitation frequency of 3 Hz with an optimal external load. The experimental results were analytically verified using the derived theoretical model. Superior performance of the harvester in terms of the figure-of-merit comparing previously reported works is demonstrated. The novelty of this work lies in the combination of an analytical modeling method and experimental validation that together can be used to increase the REWOD harvested power extensively without requiring any external bias voltage.

    

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5. Calibration sources for the LEGEND-200 experiment

   https://doi.org/10.1088/1748-0221/18/02/P02001  

   Baudis, L. ; Benato, G. ; Bond, E.M. ; Chiu, P.J. ; Elliott, S.R. ; Massarczyk, R. ; Meijer, S.J. ; Müller, Y. ( February 2023 , Journal of Instrumentation)

   Abstract In the search for a monochromatic peak as the signature of neutrinoless double beta decay an excellent energy resolution and an ultra-low background around the Q -value of the decay are essential. The LEGEND-200 experiment performs such a search with high-purity germanium detectors enriched in 76 Ge immersed in liquid argon. To determine and monitor the stability of the energy scale and resolution of the germanium diodes, custom-made, low-neutron emission 228 Th sources are regularly deployed in the vicinity of the crystals. Here we describe the production process of the 17 sources available for installation in the experiment, the measurements of their alpha- and gamma- activities, as well as the determination of the neutron emission rates with a low-background LiI(Eu) detector operated deep underground. With a flux of ( 4.27 ± 0.60 stat ± 0.92 syst ) × 10 -4  n / (kBq·s), approximately one order of magnitude below that of commercial sources, the neutron-induced background rate, mainly from the activation of 76 Ge, is negligible compared to other background sources in LEGEND-200. 

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