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Rational Phase Control in the Synthesis of Cobalt Sulfides

https://doi.org/10.1021/acs.chemmater.4c00911

Edwards, Peter_H; Bairan_Espano, Jeremy_R; Macdonald, Janet_E (July 2024, Chemistry of Materials)
Five Hypotheses on the Origins of Temperature Dependence of ⁷⁷ Se NMR Shifts in Diselenides

https://doi.org/10.1021/acs.inorgchem.4c01025

Koziel, Alexandra_C; Bortoli, Marco; Tremblay, Matthew; Zhao, Yilun; Orian, Laura; Yang, Zhongyue_J; Schley, Nathan_D; Macdonald, Janet_E (June 2024, Inorganic Chemistry)
Controlling Phase in Colloidal Synthesis

https://doi.org/10.1021/acsnanoscienceau.3c00057

Endres, Emma_J; Bairan_Espano, Jeremy_R; Koziel, Alexandra; Peng, Antony_R; Shults, Andrey_A; Macdonald, Janet_E (February 2024, ACS Nanoscience Au)
Role of carboxylates in the phase determination of metal sulfide nanoparticles

https://doi.org/10.1039/D3NH00227F

Shults, Andrey A.; Lu, Guanyu; Caldwell, Joshua D.; Macdonald, Janet E. (September 2023, Nanoscale Horizons)

At low carboxylate concentrations the sulfur source is highly reactive thiourea, which gives rise to sulfur rich nanoparticles. At high carboxylate concentrations, the sulfur source is the less reactive thiocyanate, resulting in sulfur poor phases.
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Phase Control in the Synthesis of Iron Sulfides

https://doi.org/10.1021/jacs.3c05653

Bairan Espano, Jeremy R.; Macdonald, Janet E. (August 2023, Journal of the American Chemical Society)

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