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1. Aminochronology and time averaging of Quaternary land snail assemblages from colluvial deposits in the Madeira Archipelago, Portugal

   https://doi.org/10.1017/qua.2019.1  

   New, Evan ; Yanes, Yurena ; Cameron, Robert A.D. ; Miller, Joshua H. ; Teixeira, Dinarte ; Kaufman, Darrell S. ( September 2019 , Quaternary Research)

   Abstract Understanding the properties of time averaging (age mixing) in a stratigraphic layer is essential for properly interpreting the paleofauna preserved in the geologic record. This work assesses the age and quantifies the scale and structure of time averaging of land snail-rich colluvial sediments from the Madeira Archipelago (Portugal) by dating individual shells using amino acid racemization calibrated with graphite-target and carbonate-target accelerator mass spectrometry radiocarbon methods. Gastropod shells of Actinella nitidiuscula were collected from seven sites on the volcanic islands of Bugio and Deserta Grande (Desertas Islands), where snail shells are abundant and well preserved in Quaternary colluvial deposits. Results show that the shells ranged in age from modern to ~48 cal ka BP (calibrated radiocarbon age), covering the last glacial and present interglacial periods. Snail shells retrieved from two of the colluvial sites exhibit multimillennial age mixing (>6 ka), which significantly exceeds the analytical error from dating methods and calibration. The observed multimillennial mixing of these assemblages should be taking into consideration in upcoming paleoenvironmental and paleoecological studies in the region. The extent of age mixing may also inform about the time span of colluvial deposition, which can be useful in future geomorphological studies. In addition, this studymore »presents the first carbonate-target radiocarbon results for land snail shells and suggests that this novel, rapid, and more affordable dating method offers reliable age estimates for small land snail shells younger than ~20 cal ka BP.« less
2. Oceanic cooling recorded in shells spanning the Medieval Climate Anomaly in the subtropical eastern North Atlantic Ocean

   Parker, W.G. ( January 2020 , Quaternary science reviews)

   The Medieval Climate Anomaly (MCA; 900e1300 AD) was the most recent period of pre-industrial climatic warming in the northern hemisphere, and thus estimations of MCA signals can illuminate possible impacts of anthropogenic climate change. Current high-resolution MCA climate signals are restricted to mid- and high-latitude regions, which confounds inferences of how the MCA impacted some global/hemispheric climate mechanisms (e.g. North Atlantic Oscillation; NAO). To address this knowledge gap, we estimate seasonally-resolved sea surface temperatures (SSTs) from the oxygen isotope composition (d18O) of serially sampled Phorcus atratus shells from archaeological sites spanning the MCA in the Canary Islands. Twelve archaeological and six modern P. atratus shells were analyzed, and archaeological shells were dated using carbonate-target radiocarbon dating. SSTs were estimated using the published aragonite-water equilibrium fractionation equation. Modern shells showed a mean SST of 20.0 ± 1.5
   C, with a seasonal amplitude of 5.3 ± 0.9
   C. Archaeological shells exhibited a mean SST of 18.2 ± 0.7
   C, with a mean seasonal amplitude of 5.5 ± 1.0
   C. Thus, shells that span the MCA in the Canary Islands recorded SSTs that were significantly cooler than the modern (P < .05), contrasting with warming estimates and model predictions elsewhere in the Northernmore »Hemisphere. We propose that the observed cooling resulted from increased upwelling in NW Africa due to a strengthening of the prevailing westerlies and coastal winds along the African shoreline. The intensified upwelling scenario during the MCA is partially supported by in-situ carbon isotope data (d13C) retrieved from the archaeological shells, which was compared to the d13C values of modern shells and dissolved inorganic carbon in the ambient seawater. These results are consistent with other low-latitude temperature/precipitation anomalies associated with a positive NAO mode, suggesting a transition to a positive NAO index during the middle and late MCA that possibly extended later into the 13th century AD.« less
3. IMPLICATIONS OF SINGLE-STEP GRAPHITIZATION FOR RECONSTRUCTING LATE HOLOCENE RELATIVE SEA-LEVEL USING RADIOCARBON-DATED ORGANIC COASTAL SEDIMENT

   https://doi.org/10.1017/RDC.2022.55  

   Sefton, Juliet P ; Kemp, Andrew C ; Elder, Kathryn L ; Hansman, Roberta L ; Roberts, Mark L ( October 2022 , Radiocarbon)

   ABSTRACT Late Holocene relative sea-level reconstructions are commonly generated using proxies preserved in salt-marsh and mangrove sediment. These depositional environments provide abundant material for radiocarbon dating in the form of identifiable macrofossils (salt marshes) and bulk organic sediment (mangroves). We explore if single-step graphitization of these samples in preparation for radiocarbon dating can increase the number and temporal resolution of relative sea-level reconstructions without a corresponding increase in cost. Dating of salt-marsh macrofossils from the northeastern United States and bulk mangrove sediment from the Federated States of Micronesia indicates that single-step graphitization generates radiocarbon ages that are indistinguishable from replicates prepared using traditional graphitization, but with a modest increase in error (mean/maximum of 6.25/15 additional 14 C yr for salt-marsh macrofossils). Low 12 C currents measured on bulk mangrove sediment following single-step graphitization likely render them unreliable despite their apparent accuracy. Simulated chronologies for six salt-marsh cores indicate that having twice as many radiocarbon dates (since single-step graphitization costs ∼50% of traditional graphitization) results in narrower confidence intervals for sample age estimated by age-depth models when the additional error from the single-step method is less than ∼50 14 C yr (∼30 14 C yr if the chronology also utilizes historicalmore »age markers). Since these thresholds are greater than our empirical estimates of the additional error, we conclude that adopting single-step graphitization for radiocarbon measurements on plant macrofossils is likely to increase precision of age-depth models by more than 20/10% (without/with historical age markers). This improvement can be implemented without additional cost.« less
4. Radiocarbon offsets and old world chronology as relevant to Mesopotamia, Egypt, Anatolia and Thera (Santorini)

   https://doi.org/10.1038/s41598-020-69287-2  

   Manning, Sturt W. ; Wacker, Lukas ; Büntgen, Ulf ; Bronk Ramsey, Christopher ; Dee, Michael W. ; Kromer, Bernd ; Lorentzen, Brita ; Tegel, Willy ( August 2020 , Scientific Reports)

   The new IntCal20 radiocarbon record continues decades of successful practice by employing one calibration curve as an approximation for different regions across the hemisphere. Here we investigate three radiocarbon time-series of archaeological and historical importance from the Mediterranean-Anatolian region, which indicate, or may include, offsets from IntCal20 (~0–22¹⁴C years). While modest, these differences are critical for our precise understanding of historical and environmental events across the Mediterranean Basin and Near East. Offsets towards older radiocarbon ages in Mediterranean-Anatolian wood can be explained by a divergence between high-resolution radiocarbon dates from the recent generation of accelerator mass spectrometry (AMS) versus dates from previous technologies, such as low-level gas proportional counting (LLGPC) and liquid scintillation spectrometry (LSS). However, another reason is likely differing growing season lengths and timings, which would affect the seasonal cycle of atmospheric radiocarbon concentrations recorded in different geographic zones. Understanding and correcting these offsets is key to the well-defined calendar placement of a Middle Bronze Age tree-ring chronology. This in turn resolves long-standing debate over Mesopotamian chronology in the earlier second millennium BCE. Last but not least, accurate dating is needed for any further assessment of the societal and environmental impact of the Thera/Santorini volcanic eruption.
5. A CENTENNIAL AMBIGUITY: THE CHALLENGE OF RESOLVING THE DATE OF THE JEAN-BAPTISTE LAINÉ (MANTLE), ONTARIO, SITE—AROUND AD 1500 OR AD 1600?—AND THE CASE FOR WOOD-CHARCOAL AS A TERMINUS POST QUEM

   https://doi.org/10.1017/RDC.2022.23  

   Manning, Sturt W ; Birch, Jennifer ( April 2022 , Radiocarbon)

   ABSTRACT Considered in isolation, the radiocarbon ( 14 C) dates on short-lived plant remains from the Jean-Baptiste Lainé (formerly Mantle) site, Ontario, yield an ambiguous result: more or less similar probability around AD 1500 or alternatively around AD 1600. This village site, likely of no more than ca. 20–30 years total duration, illustrates the challenges of high-resolution dating across periods with a reversal/plateau in the 14 C calibration curve. Another problem we identify is the tendency for dating probability for short-duration sites to sometimes be overly compressed as dating intensity increases under analysis with OxCal, and for probability to shift away from the real age range especially during reversal/plateau episodes. To address both issues additional constraints are necessary. While a tree-ring sequenced 14 C “wiggle-match” is the best option where available, we investigate how, in the absence of such an option, use of the in-built age in wood-charcoal samples can be used to distinguish the likely correct date range. This approach can resolve ambiguities in dating, e.g., for shorter-duration Late Woodland village sites in northeastern North America, but also other short-duration cases corresponding with reversal/plateau episodes on the 14 C calibration curve. We place the Jean-Baptiste Lainé site most likelymore »in a range between ca. AD 1595–1626 (95.4% probability).« less