skip to main content
US FlagAn official website of the United States government
dot gov icon
Official websites use .gov
A .gov website belongs to an official government organization in the United States.
https lock icon
Secure .gov websites use HTTPS
A lock ( lock ) or https:// means you've safely connected to the .gov website. Share sensitive information only on official, secure websites.


Title: The effect of cooling during deformation on recrystallized grain-size piezometry
Abstract Most exposed middle- and lower-crustal shear zones experienced deformation while cooling. We investigated the effect of the strengthening associated with such cooling on differential stress estimates based on recrystallized grain size. Typical geologic ratios of temperature change per strain unit were applied in Griggs Rig (high pressure-temperature deformation apparatus) general shear experiments on quartzite with cooling rates of 2–10 °C/h from 900 °C to 800 °C, and a shear strain rate of ∼2 × 10−5 s−1. Comparisons between these “cooling-ramp” experiments and control experiments at constant temperatures of 800 °C and 900 °C indicated that recrystallized grain size did not keep pace with evolving stress. Mean recrystallized grain sizes of the cooling-ramp experiments were twice as large as expected from the final stresses of the experiments. The traditional approach to piezometry involves a routine assumption of a steady-state microstructure, and this would underestimate the final stress during the cooling-ramp experiments by ∼40%. Recrystallized grain size in the cooling-ramp experiments is a better indicator of the average stress of the experiments (shear strains ≥3). Due to the temperature sensitivity of recrystallization processes and rock strength, the results may underrepresent the effect of cooling in natural samples. Cooling-ramp experiments produced wider and more skewed grain-size distributions than control experiments, suggesting that analyses of grain-size distributions might be used to quantify the degree to which grain size departs from steady-state values due to cooling, and thereby provide more accurate constraints on final stress.  more » « less
Award ID(s):
1833496
PAR ID:
10182622
Author(s) / Creator(s):
; ; ;
Date Published:
Journal Name:
Geology
Volume:
48
Issue:
6
ISSN:
0091-7613
Page Range / eLocation ID:
531 to 535
Format(s):
Medium: X
Sponsoring Org:
National Science Foundation
More Like this
  1. SUMMARY The occurrence of plate tectonics on Earth is rooted in the physics of lithospheric ductile weakening and shear-localization. The pervasiveness of mylonites at lithospheric shear zones is a key piece of evidence that localization correlates with reduction in mineral grain size. Most lithospheric mylonites are polymineralic and the interaction between mineral phases, such as olivine and pyroxene, especially through Zener pinning, impedes normal grain growth while possibly enhancing grain damage, both of which facilitate grain size reduction and weakening, as evident in lab experiments and field observations. The efficacy of pinning, however, relies on the mineral phases being mixed and dispersed at the grain scale, where well-mixed states lead to greater mylonitization. To model grain mixing between different phases at the continuum scale, we previously developed a theory treating grain-scale processes as diffusion between phases, but driven by imposed compressive stresses acting on the boundary between phases. Here we present a new model for shearing rock that combines our theory for diffusive grain mixing, 2-D non-Newtonian flow and two-phase grain damage. The model geometry is designed specifically for comparison to torsional shear-deformation experiments. Deformation is either forced by constant velocity or constant stress boundary conditions. As the layer is deformed, mixing zones between different mineralogical units undergo enhanced grain size reduction and weakening, especially at high strains. For constant velocity boundary experiments, stress drops towards an initial piezometric plateau by a strain of around 4; this is also typical of monophase experiments for which this initial plateau is the final steady state stress. However, polyphase experiments can undergo a second large stress drop at strains of 10–20, and which is associated with enhanced phase mixing and resultant grain size reduction and weakening. Model calculations for polyphase media with grain mixing and damage capture the experimental behaviour when damage to the interface between phases is moderately slower or less efficient than damage to the grain boundaries. Other factors such as distribution and bulk fraction of the secondary phase, as well as grain-mixing diffusivity also influence the timing of the second stress drop. For constant stress boundary conditions, the strain rate increases during weakening and localization. For a monophase medium, there is theoretically one increase in strain rate to a piezometric steady state. But for the polyphase model, the strain rate undergoes a second abrupt increase, the timing for which is again controlled by interface damage and grain mixing. The evolution of heterogeneity through mixing and deformation, and that of grain size distributions also compare well to experimental observations. In total, the comparison of theory to deformation experiments provides a framework for guiding future experiments, scaling microstructural physics to geodynamic applications and demonstrates the importance of grain mixing and damage for the formation of plate tectonic boundaries. 
    more » « less
  2. The southern Appalachian Inner Piedmont (IP) has been interpreted to represent a relict crustal escape flow system that was active during the Neoacadian (370-340 Ma) orogeny. Critical to the support of this hypothesis is the identification of both the high-temperature, rheologically weak “channel,” with crustal flow driven by relatively low differential stress, and the rheologically strong “buttress,” where deformation was driven by relatively high differential stress. Paleopiezometric analyses from southern Appalachian quartz mylonites, quartzites, and quartz-bearing pelitic rocks of the eastern Blue Ridge (EBR; buttress) and IP (channel) allow gradients of differential stress driving flow to be examined. Samples located along a transect in the EBR northwest of the Brevard fault zone (BFZ) are used to define gradients in differential stress and deformation temperatures in the proposed buttress. Preliminary results for these samples suggest that deformation temperature increased, and differential stress decreased during deformation approaching the BFZ from the northwest. Mechanisms of quartz recrystallization shift from minor grain boundary bulging and dominant subgrain rotation (SGR) in samples located away from the BFZ to dominant SGR and minor grain boundary migration (GBM) in samples in the immediate BFZ footwall. Recrystallized grain sizes in the EBR are, in almost all cases, less than 150 microns on the major axis of ellipses used to approximate grain size. In the proposed crustal channel, quartz-rich samples collected along a transect south of Rosman, NC in the Brevard and Brindle Creek thrust sheets of the IP show GBM and SGR as the dominant mechanisms of deformation, as well as a general increase in grain size into the “core” of the proposed crustal channel. Recrystallized grain sizes in the Piedmont away from the BFZ commonly exceed 500 microns. These preliminary results suggest increasing deformation temperatures and decreasing differential stresses from close to the BFZ into the Piedmont, which is consistent with increased cooling of the proposed channel proximal to the colder, stronger Blue Ridge. Ongoing piezometric analyses, combined with quartz c-axis thermometry and thermochronology, may provide additional evidence to better refine the hypothesized buttress-channel relationship. 
    more » « less
  3. null (Ed.)
    Abstract In this paper, results for SS316 L microtube experiments under combined inflation and axial loading for single and multiloading segment deformation paths are presented along with a plasticity model to predict the associated stress and strain paths. The microtube inflation/tension machine, utilized for these experiments, creates biaxial stress states by applying axial tension or compression and internal pressure simultaneously. Two types of loading paths are considered in this paper, proportional (where a single loading path with a given axial:hoop stress ratio is followed) and corner (where an initial pure loading segment, i.e., axial or hoop, is followed by a secondary loading segment in the transverse direction, i.e., either hoop or axial, respectively). The experiments are designed to produce the same final strain state under different deformation paths, resulting in different final stress states. This difference in stress state can affect the material properties of the final part, which can be varied for the intended application, e.g., biomedical hardware, while maintaining the desired geometry. The experiments are replicated in a reasonable way by a material model that combines the Hill 1948 anisotropic yield function and the Hockett–Sherby hardening law. Discussion of the grain size effects during microforming impacting the ability to achieve consistent deformation path results is included. 
    more » « less
  4. Abstract The rheology of the upper mantle impacts a variety of geodynamic processes, including postseismic deformation following great earthquakes and post-glacial rebound. The deformation of upper mantle rocks is controlled by the rheology of olivine, the most abundant upper mantle mineral. The mechanical properties of olivine at steady state are well constrained. However, the physical mechanism underlying transient creep, an evolutionary, hardening phase converging to steady state asymptotically, is still poorly understood. Here, we constrain a constitutive framework that captures transient creep and steady state creep consistently using the mechanical data from laboratory experiments on natural dunites containing at least 94% olivine under both hydrous and anhydrous conditions. The constitutive framework represents a Burgers assembly with a thermally activated nonlinear stress-versus-strain-rate relationship for the dashpots. Work hardening is obtained by the evolution of a state variable that represents internal stress. We determine the flow law parameters for dunites using a Markov chain Monte Carlo method. We find the activation energy $$430\pm 20$$ 430 ± 20   and $$250\pm 10$$ 250 ± 10  kJ/mol for dry and wet conditions, respectively, and the stress exponent $$2.0\pm 0.1$$ 2.0 ± 0.1 for both the dry and wet cases for transient creep, consistently lower than those of steady-state creep, suggesting a separate physical mechanism. For wet dunites in the grain-boundary sliding regime, the grain-size dependence is similar for transient creep and steady-state creep. The lower activation energy of transient creep could be due to a higher jog density of the corresponding soft-slip system. More experimental data are required to estimate the activation volume and water content exponent of transient creep. The constitutive relation used and its associated flow law parameters provide useful constraints for geodynamics applications. Graphical Abstract 
    more » « less
  5. Critical state and continuum plasticity theories have been used in research and engineering practice in soil and rock mechanics for decades. These theories rely on postulated relationships between material stresses and strains. Some classical postulates include coaxiality between stress and strain rates, stress–dilatancy relationships, and kinematic assumptions in shear bands. Although numerical and experimental data have quantified the strains and grain kinematics in such experiments, little data quantifying grain stresses are available. Here, we report the first-known grain stress and local strain measurements in triaxial compression tests on synthetic quartz sands using synchrotron X-ray tomography and 3D X-ray diffraction. We use these data to examine the micromechanics of shear banding, with a focus on coaxiality, stress-dilatancy, and kinematics within bands. Our results indicate the following: 1) elevated deviatoric stress, strain, and stress ratios in shear bands throughout experiments; 2) coaxial principal compressive stresses and strains throughout samples; 3) significant contraction along shear bands; 4) vanishing volumetric strain but nonvanishing stress fluctuations throughout samples at all stages of deformation. Our results provide some of the first-known in situ stress and strain measurements able to aid in critically evaluating postulates employed in continuum plasticity and strain localization theories for sands. 
    more » « less