A gas metal-directed energy deposition process was used to fabricate builds using two commercial weld fillers used in power generation applications, 16-8-2 and 316H. Microstructure stability and mechanical properties were investigated through room-temperature and elevated temperature tensile testing and creep testing at 650°C, 750°C, and 825°C. 16-8-2 exhibited reduced austenite stability which resulted in athermal martensite formation after aging at 650°C for 1000 h and strain-induced martensite formation during room-temperature tensile testing. 316H exhibited relatively higher austenite stability due to increased alloying content, resulting in no athermal martensite or strain-induced martensite. Due to lower austenite stability, ferrite formed during creep at 650°C in 16-8-2, which resulted in reduced creep life and lower creep ductility compared to 316H. At 750°C and 825°C, when ferrite is no longer thermodynamically stable, 16-8-2 exhibited longer creep life and similar creep ductility as 316H. The formation of ferrite in 16-8-2 appears to have a greater impact on creep performance than the formation of embrittling topologically close-packed phases like the σ phase, as 316H exhibited superior creep performance while predicted to form 14 vol.% σ phase at 650°C.
The Effect of Temperature on the Strain-Induced Austenite to Martensite Transformation in SS 316L During Uniaxial Tension
Controlling the microstructure of components is of interest to achieve optimal final part properties, i.e., materials by design. The manufacturing process itself can affect a material’s characteristics by changing the microstructure. For example, past research has shown that austenite to martensite phase transformation in stainless steel occurs during deformation. Temperature is known to have a significant influence on this phenomenon. In this paper, the effect of temperature on the austenitic to martensite phase transformation in SS 316L under uniaxial tension is investigated. Both a cooling system and a heat exchanger were employed in a uniaxial tension experimental setup to control the temperature. Tensile specimens were strained to fracture at four temperatures of −15, 0, 10, and 20 °C. Digital imaging correlation (DIC) and a thermal imaging camera were used for tests at 0 °C and above to capture strain and temperature data, respectively. Strain and temperature data could not be obtained at −15 °C due to the DIC paint flaking during testing. X-ray diffraction was used to measure the volume fraction of martensite in both the as-received and the tensile-tested materials.
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- Award ID(s):
- 1757371
- NSF-PAR ID:
- 10277187
- Editor(s):
- Daehn G., Cao J.
- Date Published:
- Journal Name:
- Forming the Future. The Minerals, Metals & Materials Series
- Page Range / eLocation ID:
- 1853-1862
- Format(s):
- Medium: X
- Sponsoring Org:
- National Science Foundation
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