High performance carbon fibers are widely used as fiber reinforcements in composite material systems for aerospace, automotive, and defense applications. Longitudinal tensile failure of such composite systems is a result of clustering of single fiber tensile failures occurring at the microscale, on the order of a few microns to a few hundred microns. Since fiber tensile strength at the microscale has a first order effect on composite strength, it is important to characterize the strength of single fibers at microscale gage lengths which is extremely challenging. An experimental technique based on a combination of transverse loading of single fibers under SEM with DIC is a potential approach to access microscale gage lengths. The SEM-DIC technique requires creation of uniform, random, and contrastive sub-microscale speckle pattern on the curved fiber surface for accurate strain measurements. In this paper, we investigate the formation of such sub-microscale speckle patterns on individual sized IM7 carbon fibers of nominal diameter 5.2 µm via sputter coating. Various process conditions such as working pressure, sputtering current, and coating duration are investigated for pattern creation on fiber surface using a gold-palladium (Au-Pd) target. A nanocluster type sub-microscale pattern is obtained on the fiber surface for different coating conditions. Numerical translation experiments are performed using the obtained patterns to study image correlation and identify a suitable pattern for SEM-DIC experiments. The pattern obtained at a working pressure of 120–140 mTorr with 50 mA current for a duration of 10 min is found to have an average speckle size of 53 nm and good contrast for image correlation. Rigid body translation SEM experiments for drift/distortion correction using a sized IM7 carbon fiber coated with the best patterning conditions showed that Stereo-SEM-DIC is needed for accurately characterizing fiber strain fields due to its curved surface. The effect of sputter coating on fiber tensile strength and strain is investigated via single fiber tensile tests. Results showed that there is no significant difference in the mean tensile strength and failure strain between uncoated and coated fibers (average increment in fiber diameter of ∼221 nm due to coating) at 5% significance level. SEM images of failure surfaces for uncoated and coated fibers also confirmed a tensile failure of fibers as observed for polyacrylonitrile PAN-based fibers in literature.
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Sub-microscale speckle pattern creation on single carbon fibers for in-situ DIC experiments
High performance carbon and glass fibers are widely used as reinforcements in
composite material systems for aerospace, automotive, and defense applications.
Modifications to fiber surface treatment (sizing) is one of the ways to improve the
strength of fibers and hence the overall longitudinal tensile strength of the
composite. Single fiber tensile tests at the millimeter scale are typically used to
characterize the effect of sizing on fiber strength. However, the characteristic
length-scale governing the composite failure due to a cluster of fiber breaks is in the
micro-scales. To access such micro-scale gage-lengths, we aim to employ indenters
of varying radii to transversely load fibers and use scanning electron microscope
(SEM) with digital image correlation (DIC) to measure strains at these lengthscales. The use of DIC technique requires creation of a uniform, random, and high
contrast speckle pattern on the fiber surface such as that shown in Figure 1. In this
work, we investigate the formation of sub-microscale speckle pattern on carbon
fiber surface via sputter deposition and pulsed laser deposition techniques (PLD)
using Gold-Palladium (Au-Pd) and Niobium-doped SrTiO3 (Nb:STO) targets
respectively. Different processing conditions are investigated for both sputter
deposition: sputtering current and coating duration, and PLD: number of pulses
respectively to create sub-micron scale patterns viable for micro-DIC on both sized
and unsized carbon fibers. By varying the deposition conditions and SEM-imaging
the deposited patterns on fibers, successful pattern formation at sub-micron scale is
demonstrated for both as-received sized and unsized IM7 carbon fibers of average
diameter 5.2 µm via sputter deposition and PLD respectively.
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- Award ID(s):
- 1915948
- NSF-PAR ID:
- 10310326
- Date Published:
- Journal Name:
- Proceedings of the American Society for Composites Technical Conference
- ISSN:
- 1084-7243
- Format(s):
- Medium: X
- Sponsoring Org:
- National Science Foundation
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- Free Publicly Accessible Full Text
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Accepted Manuscript1.0
- Conference Paper:
- https://doi.org/10.12783/asc36/35902
