skip to main content
US FlagAn official website of the United States government
dot gov icon
Official websites use .gov
A .gov website belongs to an official government organization in the United States.
https lock icon
Secure .gov websites use HTTPS
A lock ( lock ) or https:// means you've safely connected to the .gov website. Share sensitive information only on official, secure websites.


Title: Developing Fused Deposition Modeling Additive Manufacturing Processing Strategies for Aluminum Alloy 7075: Sample Preparation and Metallographic Characterization
Currently, no commercial aluminum 7000 series filaments are available for making aluminum parts using fused deposition modeling (FDM)-based additive manufacturing (AM). The key technical challenge associated with the FDM of aluminum alloy parts is consolidating the loosely packed alloy powders in the brown-body, separated by thin layers of surface oxides and polymer binders, into a dense structure. Classical pressing and sintering-based powder metallurgy (P/M) technologies are employed in this study to assist the development of FDM processing strategies for making strong Al7075 AM parts. Relevant FDM processing strategies, including green-body/brown-body formation and the sintering processes, are examined. The microstructures of the P/M-prepared, FDM-like Al7075 specimens are analyzed and compared with commercially available FDM 17-4 steel specimens. We explored the polymer removal and sintering strategies to minimize the pores of FDM-Al7075-sintered parts. Furthermore, the mechanisms that govern the sintering process are discussed.  more » « less
Award ID(s):
1946231 2042683
PAR ID:
10319393
Author(s) / Creator(s):
; ; ; ;
Date Published:
Journal Name:
Materials
Volume:
15
Issue:
4
ISSN:
1996-1944
Format(s):
Medium: X
Sponsoring Org:
National Science Foundation
More Like this
  1. null (Ed.)
    Binder jet 3D printing combined with post-deposition sintering is a non-beam additive manufacturing (AM) method for the creation of complex metallic structures. Binder saturation and particle morphology are two important factors affecting the quality of printed parts. Here, we investigated the effects of binder saturation on dimension accuracy, porosity, microstructure and microhardness of nickel-based alloy 625 samples made of differently atomized powders. Argon gas atomized (GA) and water atomized (WA) nickel-based alloy 625 powders were used to binder jet samples for a detailed comparative study. The optimal binder saturation for WA system is 60% to 70%, whereas for GA system the optimal is about 80%. Generally, GA samples achieved better overall quality than WA samples in terms of packing density, dimensional accuracy, sintered density, and microhardness. This difference is attributed mainly to the particle morphology including sphericity and roundness. The critical threshold for visible binder bleeding phenomenon in WA and GA systems is determined to be 120% and 140% binder saturation, respectively. Mechanisms for binder bleeding phenomenon at different saturation levels for WA and GA systems are discussed in detail. A pore evolution model is proposed to better understand the printing and sintering processes. 
    more » « less
  2. Abstract   Metal injection molding (MIM) processes are generally more cost-effective for the generation of metallic AM components. However, the thermal processing required to remove the polymer and sinter the metal powder is not well understood in terms of resulting mechanical response and damage evolution, especially in ambient atmospheres where contamination is present. This study aims to provide a range of achievable mechanical properties of copper produced using a MIM-based method called fused filament fabrication (FFF) that is post-processed in a nonideal environment. These results showed direct correlations between sintering temperature to multiple aspects of material behavior. In addition, Nondestructive Evaluation (NDE) methods are leveraged to understand the variation in damage evolution that results from the processing, and it is shown that the higher sintering temperatures provided more desirable tensile properties for strength-based applications. Moreover, these results demonstrate a potential to tailor mechanical properties of FFF manufactured copper for a specific application. 
    more » « less
  3. Additive manufacturing (AM) provides exceptional geometrical freedom to the architects and designers and enables the construction of architecturally exposed steel structures. However, the AM structural elements inherently possess microscale defects that can affect their ductility. This study aims to identify the fracture-initiating mechanism in AM 17-4 stainless steel that is popularly used owing to its excellent engineering properties. To this end, axisymmetric cylindrical notched and unnotched tension specimens are manufactured employing direct metal laser sintering from 17-4 stainless steel powder with established processing and build parameters. The test specimens were manufactured using a 90° build orientation with the build plate and a layer thickness of 40 μm. Postprocessing heat treatment was avoided as the study focused on understanding the failure mechanism in as-built AM test specimens. Detailed metallurgical analysis is performed employing scanning electron microscopy (SEM) and electron backscatter diffraction. Subsequently, micro–computed tomography (CT) studies are conducted on the tension specimens before and after mechanical testing. Although the SEM analyses of fracture surfaces are inconclusive, the micro-CT analysis revealed evidence of nucleation of new microvoids, growth of existing voids, and void coalescence in the vicinity of the fracture surface, which is unequivocal evidence for ductile fracture. Furthermore, the larger AM defects were found to play an important role in lowering the ductility in addition to stress concentration, and the fracture was initiated when the AM defects coalesced over a length of around 600 μm. The conclusions of this study emphasize the importance of controlling the maximum size of defects in AM structural elements to improve their performance. 
    more » « less
  4. Utilizing metal nanoparticles (NPs) in Additive Manufacturing (AM) enables fabricating parts with submicrometer resolution. The thermal properties of metal NPs are drastically different from their bulk and micronsize counterparts due to nanoscale thermal transport effects, e.g. ballistic phonon/electron transport instead of diffusive transport described by Fourier’s Law. Rough estimation of metal NPs’ thermal properties with bulk values will inevitably cause large errors for AM applications, because thermal properties evolve along with the sintering process. In this study, thermal properties of 100 nm Cu NPs are examined at different sintering stages. Effective density is measured between 3500 and 5300 kg/m 3 at a sintering temperature range of 100 and 400 °C, and the sintering of Cu NPs is determined to be around 300 °C using Thermogravimetry analysis (TGA) with Differential Scanning Calorimeter (DSC). A picosecond Transient Thermoreflectance (ps-TTR) technique is employed to measure the effective thermal conductivity of Cu NPs, which jumps from 18.5 ± 0.8 W/m ∙K to 26.8 ± 2.1 W/m ⋅K onset of sintering around 300 °C. These values are less than 1/10 of the bulk value (398 W/m ⋅K). The effective thermal conductivity is almost independent on porosity except in the temperature range close to 300 °C, which comes from two factors related with nanoscale thermal transport: (i) ballistic electron transport is important in particles with size comparable with electron mean free path; (ii) effective thermal conductivity is dominated by interface scattering on particles surfaces. Our results provide insights about the importance on accurate characterization of thermal properties in metal nanoparticles due to the nanoscale phenomena. 
    more » « less
  5. Surface topography represents a critical barrier to the advancement of additive manufacturing (AM). Because some internal features cannot be polished and because of the growing trend of in situ process monitoring, it is important to understand the as-built surface topography of AM components. Here we highlight the challenges of using industry-standard surface-measurement techniques on binder-jet-printed parts. We measured the topography of binder-jet-printed Inconel alloy 625 samples in their green state and over the course of sintering; this system allowed the investigation of identical starting materials undergoing systematic changes in topography. Specifically, we compared the results from industry-standard surface-measurement techniques—optical interferometry, 3D microscopy (by fringe projection), and stylus profilometry—against the “true topography,” as revealed by cross-sectional scanning electron microscopy. While the true topography changed significantly with sintering, the industry-standard techniques detected no change in the root-mean-square height because of complex surface features, including multi-scale topography, overhangs, and steep surface slopes. While these findings do not invalidate the use of industry-standard techniques for binder-jet-printed samples, they demonstrate a challenge in their application, and they motivate the development of new metrics and new techniques to more accurately describe surface topography in AM. 
    more » « less