Balancing strength and ductility is crucial for structural materials, yet often presents a paradoxical challenge. This research focuses on crafting a unique bimetallic structure, combining non-magnetic, stainless steel 316L (SS316L) with limited strength but enhanced ductility and magnetic, martensitic 17-4 PH with higher strength but lower ductility. Utilizing a powder-based laser-directed energy deposition (L-DED) system, two vertical bimetallic configurations (SS316L/17-4 PH) and a radial bimetallic structure (SS316L core encased in 17-4 PH) were fabricated. Monolithic SS316L, 17-4 PH, and a 50% SS316L/50% 17-4 PH mixture were printed. The printed samples' phase, microstructure, room temperature mechanical properties, and fracture morphology were examined in as-printed conditions. Bimetallic samples exhibited both phases, with a smooth grain transition at the interface. Radial bimetallic samples demonstrated higher mechanical strength than other compositions, except 17-4 PH. These findings showcase the potential of the L-DED approach for creating functional components with tailored mechanical properties.
more »
« less
This content will become publicly available on August 31, 2025
Additively Manufactured 17-4 PH Stainless Steels for Fracture Management Devices
Stainless steel 316L (SS316L) is widely used in fracture management devices. However, SS316L does not offer any bacterial infection resistance and can cause metal-ion sensitivity due to Ni-ions' presence. 17-4PH can emerge as a promising substitute due to the intrinsic antibacterial properties of copper, a 75% reduction in nickel content, and superior mechanical properties. SS316L and 17-4 PH were manufactured using laser-directed energy deposition (LDED). 17-4PH specimens surpassed the compressive strength of SS316L by over 150%. A static magnetic field was generated in 17-4 PH specimens to understand in vitro bone cell-material interactions. In vitro human fetal osteoblast cell culture and bacterial inhibition study using Staphylococcus aureus and Pseudomonas aeruginosa were carried out on these specimens with SS316L as control and as-processed and magnetized 17-4 PH as treatments. Results demonstrated that magnetized 17-4 PH exhibited 25% enhancement in hFOB proliferation and 70% reduction in bacterial colonization compared to SS316L.
more »
« less
- Award ID(s):
- 1934230
- NSF-PAR ID:
- 10536685
- Publisher / Repository:
- Taylor and Francis
- Date Published:
- Journal Name:
- Virtual and physical prototyping
- ISSN:
- 1745-2759
- Page Range / eLocation ID:
- 10.1080/17452759.2024.2397698
- Subject(s) / Keyword(s):
- 17-4PH Additive manufacturing 3D printing hFOB cell culture Staphylococcus aureus (S. aureus) Pseudomonas aeruginosa (P. aeruginosa).
- Format(s):
- Medium: X
- Sponsoring Org:
- National Science Foundation
More Like this
-
-
This study investigates the mechanical behavior of additively manufactured (AM) 17-4 PH (AISI 630) stainless steels and compares their behavior to traditionally produced wrought counterparts. The goal of this study is to understand the key parameters influencing AM 17-4 PH steel fatigue life under ULCF conditions and to develop simple predictive models for fatigue-life estimation in AM 17-4 steel components. In this study, both AM and traditionally produced (wrought) material samples are fatigue tested under fully reversed (R = −1) strain controlled (2–4% strain) loading and characterized using micro-hardness, x-ray diffraction, and fractography methods. Results indicate decreased fatigue life for AM specimens as compared to wrought 17-4 PH specimens due to fabrication porosity and un-melted particle defect regions which provide a mechanism for internal fracture initiation. Heat treatment processes performed in this work, to both the AM and wrought specimens, had no observable effect on ULCF behavior. Result comparisons with an existing fatigue prediction model (the Coffin–Manson universal slopes equation) demonstrated consistent over-prediction of fatigue life at applied strain amplitudes greater than 3%, likely due to inherent AM fabrication defects. An alternative empirical ULCF capacity equation is proposed herein to aid future fatigue estimations in AM 17-4 PH stainless steel components.more » « less
-
IMECE2022-88299 Midwest Engineered Systems Inc. has created a novel laser wire metal deposition process, ADDere manufacturing. ADDere has a much higher deposition rate than powder bed fusion, making it ideal for large components. In this project, the mechanical properties of ADDere printed materials were tested and compared to typical values found in ASM publications to show the quality of materials manufactured by the ADDere printing process. A detailed material analysis was performed on samples made from Ti-6Al-4V and 17-4 PH stainless steel. This work builds upon an earlier study of samples made from 17-4 PH that were produced using a single direction pattern. In this project, the 17-4 PH samples were printed in a cross hatched pattern, and testing results were compared to existing data from single direction samples of the previous research. The Ti-6Al-4V samples were created in two builds. One using the uni-directional method and the other with the crossed pattern. Testing specimens were removed from the samples using a water jet cutter and further machined into ASTM tensile bars and metallurgic mounts to perform a thorough material evaluation. The Ti-6Al-4V sample met the expected values in the ASM literature, and the cross hatched 17-4 PH exhibited a higher hardness and better microstructure than the single direction samples from the previous work. It was also observed that when the Ti64 samples were manufactured in the cross hatched pattern, the properties indicated slight improvement and more homogeneity than those printed in single layer direction. The obtained results indicate that ADDere’s printing process can produce highly refined materials that are customizable with their expected uses. This work showcases an excellent industry collaboration of an undergraduate research experience.more » « less
-
Wire arc additive manufacturing (WAAM) presents a highly promising alternative to conventional subtractive manufacturing methods to produce metallic components, particularly in the aerospace industry, where there is a demand for 17–4 precipitation-hardened (PH) stainless steel structures. This study focuses on investigating the microstructural characteristics, showing microhardness evaluations, and analyzing the tensile properties of the as-printed parts during the 17–4 PH manufacturing process at different locations and directions. The fabrication is carried out using gas metal wire arc additive manufacturing (GM-WAAM). As a result, it was found that the microstructure of the as-deposited part showed a complex configuration consisting of both finely equiaxed and coarsely formed δ-ferrite phases with vermicular and lathy morphologies. These phases were dispersed inside the martensitic matrix, while a small amount of retained austenite was also present. It was observed that the volume fraction of retained austenite (20–5%) and δ-ferrite phases (15.5–2.5%) decreased gradually from the bottom to the top of the as-deposited wall. This reduction in the fractions of these phases resulted in a progressive increase in both hardness (∼37%) and ultimate tensile strength (UTS) along the building direction. This study successfully fabricates a high-strength and ductile 17–4 PH as-printed part using WAAM. The findings provide evidence supporting the feasibility of employing WAAM for producing defect-free, high-strength components on a large scale while maintaining mechanical properties similar or better than wrought alloy 17–4 PH.more » « less
-
Abstract Extracellular vesicles (EVs) play a fundamental role in cell and infection biology and have the potential to act as biomarkers for novel diagnostic tools. In this study, we explored the in vitro impact of bacterial lipopolysaccharide administration on cell lines that represents a target for bacterial infection in the host. Administration of lipopolysaccharide at varying concentrations to A549 and BV-2 cell lines caused only modest changes in cell death, but EV numbers were significantly changed. After treatment with the highest concentration of lipopolysaccharide, EVs derived from A549 cells packaged significantly less interleukin-6 and lysosomal-associated membrane protein 1. EVs derived from BV-2 cells packaged significantly less tumor necrosis factor after administration of lipopolysaccharide concentrations of 0.1 µg/mL and 1 µg/mL. We also examined the impact of lipopolysaccharide administration on exosome biogenesis and cargo composition in BALB/c mice. Serum-isolated EVs from lipopolysaccharide-treated mice showed significantly increased lysosomal-associated membrane protein 1 and toll-like receptor 4 levels compared with EVs from control mice. In summary, this study demonstrated that EV numbers and cargo were altered using these in vitro and in vivo models of bacterial infection.more » « less