skip to main content


Title: Ultra Low-Cycle Fatigue Behavior Comparison between Additively Manufactured and Rolled 17-4 PH (AISI 630) Stainless Steels
This study investigates the mechanical behavior of additively manufactured (AM) 17-4 PH (AISI 630) stainless steels and compares their behavior to traditionally produced wrought counterparts. The goal of this study is to understand the key parameters influencing AM 17-4 PH steel fatigue life under ULCF conditions and to develop simple predictive models for fatigue-life estimation in AM 17-4 steel components. In this study, both AM and traditionally produced (wrought) material samples are fatigue tested under fully reversed (R = −1) strain controlled (2–4% strain) loading and characterized using micro-hardness, x-ray diffraction, and fractography methods. Results indicate decreased fatigue life for AM specimens as compared to wrought 17-4 PH specimens due to fabrication porosity and un-melted particle defect regions which provide a mechanism for internal fracture initiation. Heat treatment processes performed in this work, to both the AM and wrought specimens, had no observable effect on ULCF behavior. Result comparisons with an existing fatigue prediction model (the Coffin–Manson universal slopes equation) demonstrated consistent over-prediction of fatigue life at applied strain amplitudes greater than 3%, likely due to inherent AM fabrication defects. An alternative empirical ULCF capacity equation is proposed herein to aid future fatigue estimations in AM 17-4 PH stainless steel components.  more » « less
Award ID(s):
1751699
NSF-PAR ID:
10333363
Author(s) / Creator(s):
; ;
Date Published:
Journal Name:
Metals
Volume:
11
Issue:
11
ISSN:
2075-4701
Page Range / eLocation ID:
1726
Format(s):
Medium: X
Sponsoring Org:
National Science Foundation
More Like this
  1. The ability of Additive Manufacturing (AM) processes to ensure delivery of high quality metal-based components is somewhat limited by insufficient inspection capabilities. The inspection of AM parts presents particular challenges due to the design flexibility that the fabrication method affords. The nondestructive evaluation (NDE) methods employed need to be selected based on the material properties, type of possible defects, and geometry of the parts. Electromagnetic method, in particular Eddy Current (EC), is proposed for the inspections. This evaluation of EC inspection considers surface and near-surface defects in a stainless steel (SS) 17 4 PH additively manufactured sample and a SS 17 4 PH annealed plates manufactured traditionally (reference sample). The surfaces of the samples were polished using 1 micron polishing Alumina grit to achieve a mirror like surface finish. 1.02 mm (0.04”), 0.508 mm (0.02”) and 0.203 mm (0.008”) deep Electronic Discharge Machining (EDM) notches were created on the polished surface of the samples. Lift off and defect responses for both additive and reference samples were obtained using a VMEC-1 commercial instrument and a 500 kHz absolute probe. The inspection results as well as conductivity assessments for the AM sample in terms of the impedance plane signature were compared to response of similar features in the reference sample. Direct measurement of electromagnetic properties of the AM samples is required for precise inspection of the parts. Results show that quantitative comparison of the AM and traditional materials help for the development of EC technology for inspection of additively manufactured metal parts. 
    more » « less
  2. In this paper, small blocks of 17-4 PH stainless steel were manufactured via extrusion-based bound powder extrusion (BPE)/atomic diffusion additive manufacturing (ADAM) technology in two different orientations. Ultrasonic bending-fatigue and uniaxial tensile tests were carried out on the test specimens prepared from the AM blocks. Specifically, a recently-introduced small-size specimen design is employed to carry out time-efficient fatigue tests. Based on the results of the testing, the stress–life (S-N) curves were created in the very high-cycle fatigue (VHCF) regime. The effects of the printing orientation on the fatigue life and tensile strength were discussed, supported by fractography taken from the specimens’ fracture surfaces. The findings of the tensile test and the fatigue test revealed that vertically-oriented test specimens had lower ductility and a shorter fatigue life than their horizontally-oriented counterparts. The resulting S-N curves were also compared against existing data in the open literature. It is concluded that the large-sized pores (which originated from the extrusion process) along the track boundaries strongly affect the fatigue life and elongation of the AM parts. 
    more » « less
  3. The aim of this study is to experimentally investigate the fatigue behavior of additively manufactured (AM) NiTi (i.e. Nitinol) specimens and compare the results to the wrought material. Additive manufacturing is a technique in which components are fabricated in a layer-by-layer additive process using a sliced CAD model based on the desired geometry. NiTi rods were fabricated in this study using Laser Engineered Net Shaping (LENS), a Direct Laser Deposition (DLD) AM technique. Due to the high plateau stress of the as-fabricated NiTi, all the AM specimens were heat-treated to reduce their plateau stress, close to the one for the wrought material. Two different heat treatment processes, resulting in different stress plateaus, were employed to be able to compare the results in stress- and strain-based fatigue analysis. Straincontrolled constant amplitude pulsating fatigue experiments were conducted on heat-treated AM NiTi specimens at room temperature (~24°C) to investigate their cyclic deformation and fatigue behavior. Fatigue lives of AM NiTi specimens were observed to be shorter than wrought material specifically in the high cycle fatigue regime. Fractography of the fracture surface of fatigue specimens using Scanning Electron Microscopy (SEM) revealed the presence of microstructural defects such as voids, resulting from entrapped gas or lack of fusion and serving as crack initiation sites, to be the main reason for the shorter fatigue lives of AM NiTi specimens. However, the maximum stress level found to be the most influential factor in the fatigue behavior of superelastic NiTi. 
    more » « less
  4.  
    more » « less
  5. IMECE2022-88299 Midwest Engineered Systems Inc. has created a novel laser wire metal deposition process, ADDere manufacturing. ADDere has a much higher deposition rate than powder bed fusion, making it ideal for large components. In this project, the mechanical properties of ADDere printed materials were tested and compared to typical values found in ASM publications to show the quality of materials manufactured by the ADDere printing process. A detailed material analysis was performed on samples made from Ti-6Al-4V and 17-4 PH stainless steel. This work builds upon an earlier study of samples made from 17-4 PH that were produced using a single direction pattern. In this project, the 17-4 PH samples were printed in a cross hatched pattern, and testing results were compared to existing data from single direction samples of the previous research. The Ti-6Al-4V samples were created in two builds. One using the uni-directional method and the other with the crossed pattern. Testing specimens were removed from the samples using a water jet cutter and further machined into ASTM tensile bars and metallurgic mounts to perform a thorough material evaluation. The Ti-6Al-4V sample met the expected values in the ASM literature, and the cross hatched 17-4 PH exhibited a higher hardness and better microstructure than the single direction samples from the previous work. It was also observed that when the Ti64 samples were manufactured in the cross hatched pattern, the properties indicated slight improvement and more homogeneity than those printed in single layer direction. The obtained results indicate that ADDere’s printing process can produce highly refined materials that are customizable with their expected uses. This work showcases an excellent industry collaboration of an undergraduate research experience. 
    more » « less