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1. Human occupation of northern India spans the Toba super-eruption ~74,000 years ago

   https://doi.org/10.1038/s41467-020-14668-4  

   Clarkson, Chris; Harris, Clair; Li, Bo; Neudorf, Christina M.; Roberts, Richard G.; Lane, Christine; Norman, Kasih; Pal, Jagannath; Jones, Sacha; Shipton, Ceri; et al (December 2020, Nature Communications)

   Abstract India is located at a critical geographic crossroads for understanding the dispersal of Homo sapiens out of Africa and into Asia and Oceania. Here we report evidence for long-term human occupation, spanning the last ~80 thousand years, at the site of Dhaba in the Middle Son River Valley of Central India. An unchanging stone tool industry is found at Dhaba spanning the Toba eruption of ~74 ka (i.e., the Youngest Toba Tuff, YTT) bracketed between ages of 79.6 ± 3.2 and 65.2 ± 3.1 ka, with the introduction of microlithic technology ~48 ka. The lithic industry from Dhaba strongly resembles stone tool assemblages from the African Middle Stone Age (MSA) and Arabia, and the earliest artefacts from Australia, suggesting that it is likely the product of Homo sapiens as they dispersed eastward out of Africa. 

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2. Early, intensive marine resource exploitation by Middle Stone Age humans at Ysterfontein 1 rockshelter, South Africa

   https://doi.org/10.1073/pnas.2020042118  

   Niespolo, Elizabeth M.; Sharp, Warren D.; Avery, Graham; Dawson, Todd E. (April 2021, Proceedings of the National Academy of Sciences)

   Modern human behavioral innovations from the Middle Stone Age (MSA) include the earliest indicators of full coastal adaptation evidenced by shell middens, yet many MSA middens remain poorly dated. We apply²³⁰Th/U burial dating to ostrich eggshells (OES) from Ysterfontein 1 (YFT1, Western Cape, South Africa), a stratified MSA shell midden.²³⁰Th/U burial ages of YFT1 OES are relatively precise (median ± 2.7%), consistent with other age constraints, and preserve stratigraphic principles. Bayesian age–depth modeling indicates YFT1 was deposited between 119.9 to 113.1 thousand years ago (ka) (95% CI of model ages), and the entire 3.8 m thick midden may have accumulated within ∼2,300 y. Stable carbon, nitrogen, and oxygen isotopes of OES indicate that during occupation the local environment was dominated by C₃vegetation and was initially significantly wetter than at present but became drier and cooler with time. Integrating archaeological evidence with OES²³⁰Th/U ages and stable isotopes shows the following: 1) YFT1 is the oldest shell midden known, providing minimum constraints on full coastal adaptation by ∼120 ka; 2) despite rapid sea-level drop and other climatic changes during occupation, relative shellfish proportions and sizes remain similar, suggesting adaptive foraging along a changing coastline; 3) the YFT1 lithic technocomplex is similar to other west coast assemblages but distinct from potentially synchronous industries along the southern African coast, suggesting human populations were fragmented between seasonal rainfall zones; and 4) accumulation rates (up to 1.8 m/ka) are much higher than previously observed for dated, stratified MSA middens, implying more intense site occupation akin to Later Stone Age middens. 

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3. Constraining the timescales of mafic magmatism of the Central Karoo Large Igneous Province using high precision U-Pb zircon geochronology

   https://doi.org/10.25131/sajg.125.0009  

   Muedi, T.; MacLennan, S.; Szymanowski, D.; Schoene, B.; Ramezani, J.; Oalmann, J.; Linol, B. (March 2022, South African Journal of Geology)

   Abstract Recent U-Pb high-precision geochronological studies have shown rapid emplacement of the intrusive doleritic component of the Karoo Large Igneous Province (KLIP) in Southern Africa. However, these studies focused on a relatively small geographic and altitudinal region of the KLIP. Additionally, the timing of initiation of extrusive volcanism, preserved in the Drakensberg-Lesotho highlands and its relationship to the intrusive suite, has only been imprecisely constrained by Ar-Ar dates. Here, we present new high-resolution U-Pb zircon ages on dolerite sills and dykes from across the central eastern Karoo Basin (South Africa) at elevations between mean sea level and 1 560 m, as well as U-Pb detrital zircon data that can be used to estimate the maximum age of volcaniclastic deposition near the base of the extrusive component of the KLIP. Dolerite samples were taken across two areas: (1) thick dykes exposed along the coast of the Indian Ocean to ~1 600 m flanking the Drakensberg Escarpment in the Eastern Cape; and (2) sills between 20 and 220 m below surface, in a borehole core within the interior of the Karoo Basin, 400 km hinterland from the coastline. Our estimated dolerite emplacement ages span a range of ca. 80 thousand years (Kyr), between 183.122 ± 0.029/-0.061 and 183.042 ± 0.042/-0.072 million years ago (Ma), and fall within the 331 +60/-54 Kyr age range previously established for magmatism related to the KLIP, despite the marked increase in sampling coverage in terms of area and altitude in this study. Therefore, KLIP geochronology is consistent with other LIPS such as the Siberian and Deccan Traps that supports the hypothesis of rapid emplacement timescales (<1 Myr). Additionally, these data are consistent with, but better delineate that the KLIP in southern Africa appears to be ca. 500 Kyr older than the main phase of magmatism in the Ferrar LIP of Antarctica. Detrital zircons from the basal volcanic sequence of the Drakensberg Group exhibit age peaks at ca. 1 and 0.5 Ga, typical of the surrounding Namaqua-Natal and Pan-African basement rocks, as well as younger peaks at ca. 260 and 200 Ma that likely relate to source provenances from south-western Gondwana and reworking of the Karoo Supergroup sedimentary rocks. High-precision U-Pb dates of the youngest zircon grains result in a maximum depositional age for the basal pyroclastics of 185.25 ± 0.25 Ma, allowing for a ca. 2 Myr offset with the intrusive Karoo dolerite suite. 

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4. Discovery of the Youngest Toba Tuff in South Africa; Challenges of Extremely Low Abundance Cryptotephra

   Smith, E; Johnsen, R; Ren, M; Hirniak, J; Fisher, E; Campisano, C; Marean, C. (July 2021, Annual VM Goldschmidt Conference)

   null (Ed.)

   The 74 ka Youngest Toba Tuff (YTT) was discovered as cryptotephra in South African archaeological sites at Pinnacle Point (PP) 5-6N, Vleesbaai [1] and Klasies River on the Indian Ocean, and the Diepkloof Rock Shelter on the Atlantic coast nearly 750 km west of PP. The YTT eruption distributed tephra across eastern and southern Africa and provides a widespread isochron useful for dating archaeological deposits, testing age models, and precisely determining the timing of changes in human behavior. At PP, we demonstrated that the MIS 4-5 transition began just before the YTT eruption. Humans thrived both through the YTT event and the changing climate, and important changes in technology occurred just after the Toba eruption [1]. Controversy related to trapped charge age models at the Diepkloof rock shelter [2,3] were resolved by identifying YTT at a location in the stratigraphic section that confirmed the Jacobs et al. [2] model for the site, confirming that technological changes similar to those observed at PP occurred synchronously to those at Diepkloof, not substantially before as suggested by a prior published age model [3]. Processing samples with very low abundance cryptotephra, such as that found in South Africa, is a challenge and requires revision of standard laboratory techniques. Samples with high organic or clay content benefit by being treated with 10% HCl and 3% hydrogen peroxide (H2O2). This step does not degrade shard integrity or affect chemistry and is useful in separating shards from clay and organic particles allowing better recovery in heavy liquids. We also modified the heavy liquid density range from 1.95 - 2.55 to 2.2 - 2.5 g/cm3 to more effectively remove quartz and feldspar as well as biogenic silica. This density range captures shards ranging from rhyolite to dacite in composition. [1] Smith, E. I. et al. Nature 555, 511, 2018 [2] Jacobs, Z. & Roberts, R. G. Journal of Archaeological Science 63, 175-192, 2015. [3] Tribolo, C. et al. Journal of Archaeological Science 40, 3401-3411 2013. 

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5. Zircon Constraints on the Eruptive Sequence and Magma Evolution of Rhyolites at South Sister Volcano, Oregon

   https://doi.org/10.1029/2024GC011680  

   Dechert, Annika_E; Andersen, Nathan_L; Dufek, Josef; Jilly, Christine_E (August 2024, Geochemistry, Geophysics, Geosystems)

   Abstract We present²³⁰Th‐²³⁸U crystallization ages and trace element compositions for zircons spanning the late Pleistocene to Holocene rhyolite eruptive record at South Sister volcano in the central Oregon Cascade Range. Most zircon ages are between 100 and 20 ka, with very few in secular equilibrium (>350 ka). The weighted mean of zircon ages for the two oldest South Sister rhyolites, 31.5 ± 2.1 and 39.1 ± 2.4 ka, are significantly younger than the associated⁴⁰Ar/³⁹Ar ages, 47.4 ± 9.7 and 51.4 ± 9.7 ka. We propose that these⁴⁰Ar/³⁹Ar dates, performed on plagioclase separates, are compromised by a subtle amount of excess Ar and therefore the younger weighted mean zircon ages yield more reliable eruption ages. These results imply that the interval of rhyolite eruption at South Sister during the late Pleistocene was both shorter and more productive than previously thought and that eruption at South Sister initiated after Middle Sister. Compositionally, zircons from the Pleistocene rhyolites are broadly similar and show down‐temperature zircon and plagioclase crystallization trends. However, we argue that destabilized amphibole and titanite in a common mush also exert leverage on the Pleistocene zircon trace element compositions. Divergence in the Eu/Eu* ratio between the Pleistocene and Holocene lavas implies chemically distinct magma reservoirs originating from the Pleistocene rhyolite eruptive sequence and the Holocene eruptive sequence. This work suggests a higher flux of rhyolite volcanism than previously thought and characterizes magmatic storage distinctions between the Pleistocene and Holocene rhyolites, aiding in the assessment of future eruptive hazards at South Sister volcano. 

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