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A device for measuring a plurality of material properties is designed to include accurate sensors configured to consecutively obtain thermal conductivity, electrical conductivity, and Seebeck coefficient of a single sample while maintaining a vacuum or inert gas environment. Four major design factors are identified as sample-heat spreader mismatch, radiation losses, parasitic losses, and sample surface temperature variance. The design is analyzed using finite element methods for high temperature ranges up to 1000°C as well as ultra-high temperatures up to 2500°C. A temperature uncertainty of 0.46% was estimated for a sample with cold and hot sides at 905.1 and 908.5°C, respectively. The uncertainty at 1000°C was calculated to be 0.7% for a ?T of 5°C between the hot and cold sides. The thermal conductivity uncertainty was calculated to be -8.6% at ~900°C for a case with radiative gains, and +8.2% at ~1000°C for a case with radiative losses, indicating the sensitivity of the measurement to the temperature of the thermal guard in relation to the heat spreader and sample temperature. Lower limits of -17 and -13% error in thermal conductivity measurements were estimated at the ultra-high temperature of ~2500°C for a single-stage and double-stage radiation shield, respectively. It is noted that this design is not limited to electro-thermal characterization and will enable measurement of ionic conductivity and surface temperatures of energy materials under realistic operating conditions in extreme temperature environments.
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This content will become publicly available on April 7, 2026
Transient Cryothermal Vacuum Measurement and Modeling of Thermochromic Variable Emitters for Passive Space Thermal Control
This work presents the transient temperature measurement and modeling of thermochromic variable emitters using a lab-scale cryothermal vacuum test setup. A cryostat is used to provide a space-like environment with a high vacuum and an 80 K heat sink, while a custom-designed sample holder is employed to heat up the sample with transient temperature measurement. Validation with a tungsten mirror is conducted with careful calibration of heat losses as a function of sample temperature. Approaches to reduce the heat losses are discussed as well. A previously fabricated variable emitter made of thermochromic [Formula: see text] thin film in a Fabry–Perot nanophotonic structure, whose infrared emittance increases with temperature upon [Formula: see text] insulator-to-metal phase transition, is experimentally tested at different heating power inputs. A transient heat transfer model is also developed to validate the measurements, and a thermal homeostasis effect with reduced temperature swing from the variable emitter is predicted in comparison to a commonly used static emitter. This novel cryothermal vacuum test platform would facilitate the lab-scale thermal testing of novel variable-emittance coatings for space heat control applications.
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- Award ID(s):
- 2212342
- PAR ID:
- 10636664
- Publisher / Repository:
- AIAA
- Date Published:
- Journal Name:
- Journal of Thermophysics and Heat Transfer
- ISSN:
- 0887-8722
- Page Range / eLocation ID:
- 1 to 7
- Format(s):
- Medium: X
- Sponsoring Org:
- National Science Foundation
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