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null (Ed.)The title ketenylidene, [Au 3 (C 2 O)(C 26 H 35 O 2 P) 3 ](C 2 F 6 NO 4 S 2 ), was obtained upon exposure of [2-(dicyclohexylphosphino)-2′,6′-dimethoxy-1,1′-biphenyl]gold(I) bis(trifluoromethanesulfonyl)imide to acetic anhydride at elevated temperature. The ketenylidene bridge caps the tri-gold cluster. The title compound has provided crystals that upon analysis represent the first tri-gold ketenylidene with atomic distances indicative of bonding interaction between the gold atoms.more » « less
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Anderson, Carolyn E. ; Bos, Haleigh I. ; Dreher, Daniel M. ; Hartgerink, Colin T. ; Scholtens, Chase J. ; Staples, Richard J. ( , The Journal of Organic Chemistry)Miller, S. (Ed.)Two new complementary Au(I)-catalyzed methods for the preparation of ester-substituted indolizines from easily accessible 2-propargyloxypyridines and either acetoacetates or dimethyl malonate are reported. These reactions tolerate a wide range of functionality, allowing for diversification at three distinct positions of the product (R, R1, R2). For electron-poor substrates, the highest yields are observed upon reaction with acetoacetates, while neutral and electron-rich substrates give higher yields upon treatment with dimethyl malonate.more » « less
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Rossler, Matthew D. ; Hartgerink, Colin T. ; Zerull, Emily E. ; Boss, Benjamin L. ; Frndak, Abigail K. ; Mason, Miles M. ; Nickerson, Leslie A. ; Romero, Evan O. ; Van de Burg, Jaimie E. ; Staples, Richard J. ; et al ( , Organic Letters)