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  1. This work describes a method in which the digital image correlation (DIC) method and finite element analysis (FEA) were used to create a quasi-static mixed-mode fracture envelope for bonded joints consisting of 2024-T3 Al adherends and a tough structural epoxy adhesive. Symmetric and asymmetric versions of double cantilever beam, single-leg bend, and end-notched flexure tests are used to populate the mixed-mode fracture envelope with results at several mode mixities. Experiments are conducted in a universal testing machine while recording images for subsequent DIC analysis. Finite element analysis is used to implement cohesive zone models (CZMs) of the adhesive fracture and to account for plastic deformation of adherends. Mode I and mode II traction separation laws (TSLs) are determined from a property identification method with a Benzeggagh–Kenane mixed-mode coupling law used to model mixed-mode behavior. FEA results are shown to provide a good agreement to both the crosshead displacement and DIC data. The methods in this paper serve as a potential framework for future calibration of mixed-mode fracture envelopes for joints bonded with very tough adhesives that complicate assessment with traditional data analysis methods. 
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  2. The viscoelastic properties of carbon fiber reinforced thermoset composites are of utmost importance during processing such materials using composite forming. The quality of the manufactured parts is largely dependent on intelligent process parameter selection based on the viscoelastic and flow properties of the polymer resin. Viscoelastic properties such as the complex viscosity (η*), storage modulus (G'), loss modulus (G''), and loss tangent (tanδ) are used to determine the critical transition events (such as gelation) during curing. An understanding of the changes in viscoelastic properties as a function of processing temperature and degree of cure provides insight to establish a suitable processing range for compression forming of prepreg systems. However, tracking viscoelastic properties as a function of cure during the forming process is a challenging task. In this current work, we have investigated the effect of sample size and adhesive type on the rheological properties of a commercially available carbon fiber prepreg material. Specifically, determining the linear viscoelastic region (LVE) as a function of sample configuration and different adhesive chemistries were explored. The results suggest that the square-shaped sample geometries coupled with cyanoacrylate based adhesive are optimum for conducting rheological characterization on the carbon fiber prepreg system. 
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  3. In automated layup manufacturing processes of fiber-reinforced polymer composites, the quality of the manufactured part is strongly dependent on frictional behavior. Improper control of frictional forces can lead to defect formation. Frictional sliding rheometry tests provide an innovative methodology to accurately characterize the tool-ply friction of unidirectional (UD) prepreg employing unique annular plate geometries. The effect of processing parameters (temperature, velocity, and normal force) on the frictional response of a carbon fiber prepreg was studied. Moreover, utilizing custom designed plate geometries coupled with optically transparent fixtures allowed for in-situ quantification of the prepreg-rigid surface contact area along with simultaneous characterization of the process parameter-dependent frictional mechanisms. Our findings highlight the reduction in frictional forces with increasing temperature, attributed to the increased resin flowability, while increases in sliding rates resulted in a pronounced increase in the frictional forces. The effect of applied load on the frictional characteristics was more complicated due to contributions from both the adhesive and normal forces. Finally, the results were interpreted in light of the contact area measurements performed at different temperatures, normal force, and sliding rate. 
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