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  • Synthesis and Characterization of Single-Phase Metal Dodecaboride Solid Solutions: Zr 1–x Y x B 12 and Zr 1–x U x B 12
Title: Synthesis and Characterization of Single-Phase Metal Dodecaboride Solid Solutions: Zr 1–x Y x B 12 and Zr 1–x U x B 12
Award ID(s):
1809116
PAR ID:
10101108
Author(s) / Creator(s):
; ; ; ; ; ; ; ; ; ; ; ; ;
Date Published:
Journal Name:
Journal of the American Chemical Society
Volume:
141
Issue:
22
ISSN:
0002-7863
Page Range / eLocation ID:
9047 to 9062
Format(s):
Medium: X
Sponsoring Org:
National Science Foundation
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    We synthesized a series of Zr1−xTixS3solid solutions (0 ≤x≤ 1)viaa direct reaction between Zr–Ti alloys and sulfur vapor at 600 °C. These solid solutions have a tunable bandgap in the 1–2 eV range that linearly increases with the Zr content. 
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    Alloyed Ba(Zr1−xTix)S3nanoparticles are preparedviaa solution-phase route. The phase evolution from a chalcogenide perovskite phase at lowxto a hexagonal non-perovskite phase at highxis tracked along with changes in the optical properties. 
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