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1. 2D material programming for 3D shaping

   https://doi.org/10.1038/s41467-021-20934-w  

   Nojoomi, Amirali; Jeon, Junha; Yum, Kyungsuk (December 2021, Nature Communications)

   null (Ed.)

   Abstract Two-dimensional (2D) growth-induced 3D shaping enables shape-morphing materials for diverse applications. However, quantitative design of 2D growth for arbitrary 3D shapes remains challenging. Here we show a 2D material programming approach for 3D shaping, which prints hydrogel sheets encoded with spatially controlled in-plane growth (contraction) and transforms them to programmed 3D structures. We design 2D growth for target 3D shapes via conformal flattening. We introduce the concept of cone singularities to increase the accessible space of 3D shapes. For active shape selection, we encode shape-guiding modules in growth that direct shape morphing toward target shapes among isometric configurations. Our flexible 2D printing process enables the formation of multimaterial 3D structures. We demonstrate the ability to create 3D structures with a variety of morphologies, including automobiles, batoid fish, and real human face. 

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2. Leveraging Monostable and Bistable Pre‐Curved Bilayer Actuators for High‐Performance Multitask Soft Robots

   https://doi.org/10.1002/admt.202000370  

   Chi, Yinding; Tang, Yichao; Liu, Haijun; Yin, Jie (June 2020, Advanced Materials Technologies)

   Soft actuators are typically designed to be inherently stress‐free and stable. Relaxing such a design constraint allows exploration of harnessing mechanical prestress and elastic instability to achieve potential high‐performance soft robots. Here, the strategy of prestrain relaxation is leveraged to design pre‐curved soft actuators in 2D and 3D with tunable monostability and bistability that can be implemented for multifunctional soft robotics. By bonding stress‐free active layer with embedded pneumatic channels to a uniaxially or biaxially pre‐stretched elastomeric strip or disk, pre‐curved 2D beam‐like bending actuators and 3D doming actuators are generated after prestrain release, respectively. Such pre‐curved soft actuators exhibit tunable monostable and bistable behavior under actuation by simply manipulating the prestrain and the biased bilayer thickness ratio. Their implications in multifunctional soft robotics are demonstrated in achieving high performance in manipulation and locomotion, including energy‐efficient soft gripper to holding objects through prestress, fast‐speed larva‐like jumping soft crawler with average locomotion speed of 0.65 body‐length s−1 (51.4 mm s−1), and fast swimming bistable jellyfish‐like soft robot with an average speed of 53.3 mm s−1. 

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3. Design of Bistable Soft Deployable Structures via a Kirigami‐Inspired Planar Fabrication Approach

   https://doi.org/10.1002/admt.202300088  

   Mungekar, Mrunmayi; Ma, Leixin; Yan, Wenzhong; Kackar, Vishal; Shokrzadeh, Shyan; Jawed, Mohammad Khalid (January 2023, Advanced Materials Technologies)

   Fully soft bistable mechanisms have shown extensive applications ranging from soft robotics, wearable devices, and medical tools, to energy harvesting. However, the lack of design and fabrication methods that are easy and potentially scalable limits their further adoption into mainstream applications. Herein, a top–down planar approach is presented by introducing Kirigami-inspired engineering combined with a pre-stretching process. Using this method, Kirigami-Pre-stretched Substrate-Kirigami trilayered precursors are created in a planar manner; upon release, the strain mismatch—due to the pre-stretching of substrate—between layers will induce an out-of-plane buckling to achieve targeted 3D bistable structures. By combining experimental characterization, analytical modeling, and finite element simulation, the effect of the pattern size of Kirigami layers and pre-stretching on the geometry and stability of resulting 3D composites is explored. In addition, methods to realize soft bistable structures with arbitrary shapes and soft composites with multistable configurations are investigated, which may encourage further applications. This method is demonstrated by using bistable soft Kirigami composites to construct two soft machines: (i) a bistable soft gripper that can gently grasp delicate objects with different shapes and sizes and (ii) a flytrap-inspired robot that can autonomously detect and capture objects. 

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4. Rapid Design of Fully Soft Deployable Structures Via Kirigami Cuts and Active Learning

   https://doi.org/10.1002/admt.202301305  

   Ma, Leixin; Mungekar, Mrunmayi; Roychowdhury, Vwani; Jawed, MK (March 2024, Advanced Materials Technologies)

   Soft deployable structures – unlike conventional piecewise rigid deployables based on hinges and springs – can assume intricate 3‐D shapes, thereby enabling transformative soft robotic and manufacturing technologies. Their virtually infinite degrees of freedom allow precise control over the final shape. The same enabling high dimensionality, however, poses a challenge for solving the inverse problem: fabrication of desired 3D structures requires manufacturing technologies with extensive local actuation and control, and a trial‐and‐error search over a large design space. Both of these shortcomings are addressed by first developing a simplified planar fabrication approach that combines two ingredients: strain mismatch between two layers of a composite shell and kirigami cuts that relieves localized stress. In principle, it is possible to generate targeted 3‐D shapes by designing the appropriate kirigami cuts and the amount of prestretch (without any local control). Second, a data‐driven physics‐guided framework is formulated that reduces the dimensionality of the inverse design problem using autoencoders and efficiently searches through the “latent” parameter space in an active learning approach. The rapid design procedure is demonstrated via a range of target shapes, such as peanuts, pringles, flowers, and pyramids. Experiments and our numerical predictions are found to be in good agreement. 

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5. Self‐Assembly for Creating Vertically‐Aligned Graphene Micro Helices with Monolayer Graphene as Chiral Metamaterials

   https://doi.org/10.1002/adma.202401451  

   Lin, Zihao; Mikhael, Carol; Dai, Chunhui; Cho, Jeong‐Hyun (April 2024, Advanced Materials)

   Abstract Graphene's emergence enables creating chiral metamaterials in helical shapes for terahertz (THz) applications, overcoming material limitations. However, practical implementation remains theoretical due to fabrication challenges. This paper introduces a dual‐component self‐assembly technique that enables creating vertically‐aligned continuous monolayer graphene helices at microscale with great flexibility and high controllability. This assembly process not only facilitates the creation of 3D microstructures, but also positions the 3D structures from a horizontal to a vertical orientation, achieving an aspect ratio (height/width) of ≈2700. As a result, an array of vertically‐aligned graphene helices is formed, reaching up to 4 mm in height, which is equivalent to 4 million times the height of monolayer graphene. The benefit of these 3D chiral structures made from graphene is their capability to infinitely extend in height, interacting with light in ways that are not possible with traditional 2D layering methods. Such an impressive height elevates a level of interaction with light that far surpasses what is achievable with traditional 2D layering methods, resulting in a notable enhancement of optical chirality properties. This approach is applicable to various 2D materials, promising advancements in innovative research and diverse applications across fields. 

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