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1. A study of events with photoelectric emission in the DarkSide-50 liquid argon Time Projection Chamber

   The DarkSide-50 Collaboration) Agnes, P.; Albuquerque, I. F.; Alexander, T.; Alton, A. K.; Ave, M.; Back, H. O.; Batignani, G.; Biery, K.; Bocci, V.; Bonivento, W. M.; et al (July 2021, ArXivorg)

   null (Ed.)

   Finding unambiguous evidence of dark matter interactions in a particle detector is a main objective of physics research. The liquid argon time projection chamber technique for the detection of Weakly Interacting Massive Particles (WIMP) allows sensitivities down to the so-called neutrino floor for high and low WIMP masses. Based on the successful operation of the DarkSide-50 detector, a new and more sensitive experiment, DarkSide-20k, was designed and is now under construction. A thorough understanding of the DarkSide-50 detector response to events classified as dark matter as well as all other interactions is essential for an optimal design of the new experiment. In this paper, we report on a particular set of events, for which scintillation-ionization signals are observed in association with signals from single or few isolated electrons. We identified and provided an interpretation for two event types in which electrons are produced via photoelectric effect on the cathode electrode and in the bulk liquid. Events with photoelectric emissions are observed in association with most interactions with large energy depositions in the detector. From the measured rate of these events, we determine the photo-ionization probability, or photoelectric quantum efficiency, of tetraphenyl butadiene (TPB) at wavelengths around 128 nm. 

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2. Quality assurance and quality control of the $$26~\text {m}^2$$ SiPM production for the DarkSide-20k dark matter experiment

   https://doi.org/10.1140/epjc/s10052-025-14196-9  

   Acerbi, F; Adhikari, P; Agnes, P; Ahmad, I; Albergo, S; Albuquerque, I F; Alexander, T; Alton, A K; Amaudruz, P; Angiolilli, M; et al (May 2025, The European Physical Journal C)

   Abstract DarkSide-20k is a novel liquid argon dark matter detector currently under construction at the Laboratori Nazionali del Gran Sasso (LNGS) of the Istituto Nazionale di Fisica Nucleare (INFN) that will push the sensitivity for Weakly Interacting Massive Particle (WIMP) detection into the neutrino fog. The core of the apparatus is a dual-phase Time Projection Chamber (TPC), filled with 50 tonnes of low radioactivity underground argon (UAr) acting as the WIMP target. NUV-HD-cryo Silicon Photomultipliers (SiPM)s designed by Fondazione Bruno Kessler (FBK) (Trento, Italy) were selected as the photon sensors covering two$$10.5~\text {m}^2$$ $10.5{\text{m}}^2$Optical Planes, one at each end of the TPC, and a total of$$5~\text {m}^2$$ $5{\text{m}}^2$photosensitive surface for the liquid argon veto detectors. This paper describes the Quality Assurance and Quality Control (QA/QC) plan and procedures accompanying the production of FBK NUV-HD-cryo SiPM wafers manufactured by LFoundry s.r.l. (Avezzano, AQ, Italy). SiPM characteristics are measured at 77 K at the wafer level with a custom-designed probe station. As of March 2025, 1314 of the 1400 production wafers (94% of the total) for DarkSide-20k were tested. The wafer yield is$$93.2\pm 2.5$$ $93.2\pm 2.5$%, which exceeds the 80% specification defined in the original DarkSide-20k production plan. 

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3. The underground argon project: procurement and purification of argon for dark matter searches and beyond

   https://doi.org/10.3389/fphy.2024.1387069  

   Agnes, P; Back, H O; Bonivento, W; Boulay, M G; Canci, N; Caravati, M; Cebrian, S; Cocco, V; Diaz_Mairena, D; Franco, D; et al (December 2024, Frontiers in Physics)

   The existence of dark matter in the universe is inferred from abundant astrophysical and cosmological observations. The Global Argon Dark Matter Collaboration (GADMC) aims to perform the searches for dark matter in the form of weakly interacting massive particles (WIMPs), whose collisions with argon nuclei would produce nuclear recoils with tens of keV energy. Argon has been considered an excellent medium for the direct detection of WIMPs as argon-based scintillation detectors can make use of pulse shape discrimination (PSD) to separate WIMP-induced nuclear recoil signals from electron recoil backgrounds with extremely high efficiency. However, argon-based direct dark matter searches must confront the presence of intrinsic³⁹Ar as the predominant source of electron recoil backgrounds (it is a beta-emitter with an endpoint energy of 565 keV and half-life of 269 years). Even with PSD, the³⁹Ar activity in atmospheric argon (AAr), mainly produced and maintained by cosmic ray-induced nuclear reactions, limits the ultimate size of argon-based detectors and restricts their ability to probe very-low-energy events. The discovery of argon from deep underground wells with significantly less³⁹Ar than that in AAr was an important step in the development of direct dark matter detection experiments using argon as the active target. Thanks to pioneering research and successful R&D, in 2012, the first 160 kg batch of underground argon (UAr) was extracted from a CO₂well in Cortez, Colorado. The DarkSide-50 experiment at the Gran Sasso National Laboratory (LNGS) in Italy, the first liquid argon detector ever operated with a UAr target, demonstrated a ∼ 1,400 suppression of the³⁹Ar activity with respect to the atmospheric argon. An even larger suppression is expected for⁴²Ar (another intrinsic beta-emitter with the⁴²K daughter isotope, also a beta-emitter) as its production is expected mainly in the upper atmosphere. Following the results of DarkSide-50, the GADMC initiated the UAr project for extraction from underground and cryogenic purification of 100 t of argon to be used as a target in the next-generation experiment DarkSide-20k. This paper contains a description of the Urania Plant in Cortez, Colorado, where UAr is extracted; the Aria Plant in Sardinia, Italy, an industrial-scale plant comprising a 350-m state-of-the-art cryogenic isotopic distillation column, designed for further purification of the extracted argon and further reduction of the isotopic abundance of³⁹Ar; and DArT, a facility for UAr radiopurity qualification at the Canfranc Underground Laboratory (LSC), Spain. Moreover, the high radiopurity of UAr leads to other possible applications, for instance, for those neutrinoless double-beta decay experiments using argon as shielding material or, more generally, for all those activities on argon-based detectors in high-energy physics or nuclear physics, which will be briefly discussed. 

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4. Measurement of isotopic separation of argon with the prototype of the cryogenic distillation plant Aria for dark matter searches

   https://doi.org/10.1140/epjc/s10052-023-11430-0  

   Aaron, E.; Agnes, P.; Ahmad, I.; Albergo, S.; Albuquerque, I. F.; Alexander, T.; Alton, A. K.; Amaudruz, P.; Atzori Corona, M.; Ave, M.; et al (May 2023, The European Physical Journal C)

   Abstract The Aria cryogenic distillation plant, located in Sardinia, Italy, is a key component of the DarkSide-20k experimental program for WIMP dark matter searches at the INFN Laboratori Nazionali del Gran Sasso, Italy. Aria is designed to purify the argon, extracted from underground wells in Colorado, USA, and used as the DarkSide-20k target material, to detector-grade quality. In this paper, we report the first measurement of argon isotopic separation by distillation with the 26 m tall Aria prototype. We discuss the measurement of the operating parameters of the column and the observation of the simultaneous separation of the three stable argon isotopes: $${}^{36}\hbox {Ar}$$ 36 Ar , $${}^{38}\textrm{Ar}$$ 38 Ar , and $${}^{40}\textrm{Ar}$$ 40 Ar . We also provide a detailed comparison of the experimental results with commercial process simulation software. This measurement of isotopic separation of argon is a significant achievement for the project, building on the success of the initial demonstration of isotopic separation of nitrogen using the same equipment in 2019. 

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5. Constraints on directionality effect of nuclear recoils in a liquid argon time projection chamber

   https://doi.org/10.1140/epjc/s10052-023-12312-1  

   DarkSide-20k_Collaboration; Agnes, P.; Ahmad, I.; Albergo, S.; Albuquerque, I_F_M; Alexander, T.; Alton, A_K; Amaudruz, P.; Corona, M_Atzori; Ave, M.; et al (January 2024, The European Physical Journal C)

   Abstract The direct search for dark matter in the form of weakly interacting massive particles (WIMP) is performed by detecting nuclear recoils produced in a target material from the WIMP elastic scattering. The experimental identification of the direction of the WIMP-induced nuclear recoils is a crucial asset in this field, as it enables unmistakable modulation signatures for dark matter. The Recoil Directionality (ReD) experiment was designed to probe for such directional sensitivity in argon dual-phase time projection chambers (TPC), that are widely considered for current and future direct dark matter searches. The TPC of ReD was irradiated with neutrons at the INFN Laboratori Nazionali del Sud. Data were taken with nuclear recoils of known directions and kinetic energy of 72 keV, which is within the range of interest for WIMP-induced signals in argon. The direction-dependent liquid argon charge recombination model by Cataudella et al. was adopted and a likelihood statistical analysis was performed, which gave no indications of significant dependence of the detector response to the recoil direction. The aspect ratioRof the initial ionization cloud is$$R < 1.072$$ $R<1.072$with 90 % confidence level. 

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