The aim of this study is to experimentally investigate the fatigue behavior of additively manufactured (AM) NiTi (i.e. Nitinol) specimens and compare the results to the wrought material. Additive manufacturing is a technique in which components are fabricated in a layer-by-layer additive process using a sliced CAD model based on the desired geometry. NiTi rods were fabricated in this study using Laser Engineered Net Shaping (LENS), a Direct Laser Deposition (DLD) AM technique. Due to the high plateau stress of the as-fabricated NiTi, all the AM specimens were heat-treated to reduce their plateau stress, close to the one for the wrought material. Two different heat treatment processes, resulting in different stress plateaus, were employed to be able to compare the results in stress- and strain-based fatigue analysis. Straincontrolled constant amplitude pulsating fatigue experiments were conducted on heat-treated AM NiTi specimens at room temperature (~24°C) to investigate their cyclic deformation and fatigue behavior. Fatigue lives of AM NiTi specimens were observed to be shorter than wrought material specifically in the high cycle fatigue regime. Fractography of the fracture surface of fatigue specimens using Scanning Electron Microscopy (SEM) revealed the presence of microstructural defects such as voids, resulting from entrapped gas or lack of fusion and serving as crack initiation sites, to be the main reason for the shorter fatigue lives of AM NiTi specimens. However, the maximum stress level found to be the most influential factor in the fatigue behavior of superelastic NiTi.
more »
« less
This content will become publicly available on June 10, 2026
Fatigue Criticality Assessment of Volumetric Defects in Notched Specimens: A Non‐Destructive Approach
ABSTRACT This study utilizes linear elastic fracture mechanics to assess the fatigue criticality of volumetric defects in notched specimens with varying geometries. Contrasting to the existing literature, this study assesses the fatigue criticality of defects, prior to fracture, via a non‐destructive inspection technique, that is, X‐ray computed tomography (XCT). Treating volumetric defects as cracks, based on Murakami's definition, the approach calculates their Mode‐I stress intensity factor (SIF) with their local stresses obtained via linear elastic finite element analysis and utilizes the SIF to represent their criticality. For validation, cylindrical and flat specimens with notch root radii of 5 and 50 mm of AlSi10Mg and 17‐4 precipitation hardened stainless steel were fabricated, XCT scanned, and tested under fatigue loading. All crack initiating defects, observed from fractography, fell within the 99.3 percentile of the defects with the highest stress intensity factor in the respective specimens.
more »
« less
- Award ID(s):
- 2319690
- PAR ID:
- 10600155
- Publisher / Repository:
- Wiley-Blackwell
- Date Published:
- Journal Name:
- Fatigue & Fracture of Engineering Materials & Structures
- ISSN:
- 8756-758X
- Format(s):
- Medium: X
- Sponsoring Org:
- National Science Foundation
More Like this
-
-
Adhesive-bonding has become increasingly adopted for multi-material lightweight applications (e.g., automotive structures). There is a growing interest in understanding the fatigue behaviors in this type of joint for supporting structural durability modeling in practice. In this paper, an analytical fracture mechanics modeling procedure is presented in the context of a generalized sandwich specimen. Its closed form stress intensity factor solutions were then derived and applied for the correlating fatigue test data obtained from the lap-shear and coach-peel test specimens with demonstrated effectiveness. Some important implications of these analytical solutions on joint design are also discussed.more » « less
-
Electron Beam Melting (EBM) is a widespread additive manufacturing technology for metallic-part fabrication; however, final products can contain microstructural defects that reduce fatigue performance. While the effects of gas and keyhole pores are well characterized, other defects, including lack of fusion and smooth facets, warrant additional investigation given their potential to significantly impact fatigue life. Therefore, such defects were intentionally induced into EBM Ti-6Al-4V, a prevalent titanium alloy, to investigate their degradation on stress-controlled fatigue life. The focus offset processing parameter was varied outside of typical manufacturing settings to generate a variety of defect types, and specimens were tested under fatigue loading, followed by surface and microstructure characterization. Fatigue damage primarily initiated at smooth facet sites or sites consisting of un-melted powder due to a lack of fusion, and an increase in both fatigue life and void content with increasing focus offset was noted. This counter-intuitive relationship is attributed to lower focus offsets producing a microstructure more prone to smooth facets, discussed in the literature as being due to lack of fusion or cleavage fracture, and this study indicates that these smooth flaws are most likely a result of lack of fusion.more » « less
-
Abstract The cold sintering process (CSP) is a low temperature processing technique that utilizes a transient phase to synthesize dense ceramics. However, some CSP parts contain microflaws that arise due to inhomogeneities in pressure, temperature, and transient phase. This work uses 20 MHz ultrasound to verify the presence of defects in CSP ZnO samples of varying densities (84%–97%). Acoustic metrics used in this work include wave speed, which is affected by differences in the effective elastic properties of the medium, and attenuation, which quantifies wave energy loss due to scattering from defects. Wave speed maps were inhomogeneous, suggesting density gradients which were verified with scanning electron microscopy. In addition, it was demonstrated that the pores produced by cold sintering are anisometric, which increases the anisotropy in the elastic properties. High attenuation regions (>300 Np/m) are present in all samples independent of relative density and correspond to defects identified in X‐ray computed tomography (XCT) which were as small as 38 µm in effective diameter. However, some high attenuation spots do not correspond to visible defects in XCT, which suggests the presence of features undetectable with XCT such as residual secondary phases at the grain boundaries.more » « less
-
ABSTRACT We investigate the appropriateness of calving or crevasse models from the literature using linear elastic fracture mechanics (LEFM). To this end, we compare LEFM model-predicted stress intensity factors (SIFs) against numerically computed SIFs using the displacement correlation method in conjunction with the finite element method. We present several benchmark simulations wherein we calculate the SIF at the tips of water-filled surface and basal crevasses penetrating through rectangular ice slabs under different boundary conditions, including grounded and floating conditions. Our simulation results indicate that the basal boundary condition significantly influences the SIF at the crevasse tips. We find that the existing calving models using LEFM are not generally accurate for evaluating SIFs in grounded glaciers or floating ice shelves. We also illustrate that using the ‘single edge crack’ weight function in the LEFM formulations may be appropriate for predicting calving from floating ice shelves, owing to the low fracture toughness of ice; whereas, using the ‘double edge crack’ or ‘central through crack’ weight functions is more appropriate for predicting calving from grounded glaciers. To conclude, we recommend using the displacement correlation method for SIF evaluation in real glaciers and ice shelves with complex geometries and boundary conditions.more » « less
An official website of the United States government
