The current work studies the correlations between microstructure and retained austenite (RA) transformation, in a single-quenched and partitioned (Q&P) 1180 steel microstructure, through in situ tensile tests combined with electron backscatter diffraction (EBSD) analysis. This allows the study of RA stability across a limited range of morphological characteristics to be studied in the absence of confounding factors introduced by varying the entire steel microstructure. Among the microstructural attributes of interest, RA grain aspect ratio is found to have the largest influence on transformation rate, where globular-shaped grains transform more slowly than those with a more lenticular shape. Furthermore, by tracking individual grains during deformation, it is apparent that larger grains transformed more slowly than smaller grains; a purely statistical study of grain size vs strain might conclude that smaller grains are more stable, but in reality, the smaller grains transform faster and are simply statistically replaced by partially transformed larger grains. These conclusions are in contrast to relationships that might be inferred from previous studies where the entire steel microstructure was varied, along with the morphology of the RA.
more »
« less
This content will become publicly available on March 1, 2026
Effect of Strain Path on Retained Austenite Transformation Rates and Material Ductility in Transformation-Induced Plasticity-Assisted Advanced High-Strength Steel
TBF 1180 steel was plastically deformed under different strain paths in order to study both the ductility and RA transformation rates. Specimens were prepared from a 1 mm thick sheet and then tested incrementally under uniaxial tension, plane-strain tension, and biaxial tension. The retained austenite (RA) levels were measured, as a function of the plastic strain, using electron backscatter diffraction (EBSD). The plane-strain tension specimens had the fastest rate of RA transformation as a function of strain, followed by uniaxial tension, and then biaxial tension. The forming limits were measured for each strain path, yielding major limit strains of 0.12 under uniaxial tension, 0.09 under plane-strain tension, and 0.16 under biaxial tension. These results were compared to prior work on a 1.2 mm Q&P 1180 steel sheet, which had a similar yield and ultimate tensile strength, but exhibited slightly greater forming limits than the TBF material. The visual inspection of the micrographs appeared to show an equiaxed RA morphology in the Q&P 1180 steel and a mixture of equiaxed and lamellar RA grains in the TBF 1180 steel. However, the statistics generated by EBSD revealed that both alloys had RA grains with essentially the same aspect ratios. The average RA grain size in the Q&P alloy was found to be about three times larger than that of the TBF alloy. As such, the small but consistent formability advantage exhibited by the Q&P 1180 alloy along all three strain paths can be attributed to its larger average RA grain size, where larger RA grain sizes correlated with a more gradual transformation rate.
more »
« less
- Award ID(s):
- 2147126
- PAR ID:
- 10627288
- Publisher / Repository:
- MDPI
- Date Published:
- Journal Name:
- Journal of Manufacturing and Materials Processing
- Volume:
- 9
- Issue:
- 3
- ISSN:
- 2504-4494
- Page Range / eLocation ID:
- 75
- Format(s):
- Medium: X
- Sponsoring Org:
- National Science Foundation
More Like this
-
-
null (Ed.)Continuous bending under tension (CBT) is known to achieve elongation-to-failure well above that achieved under a conventional uniaxial simple tension (ST) strain path. However, the detailed mechanism for supplying this increased ductility has not been fully understood. It is clear that the necking that occurs in a typical ST specimen is avoided by constantly moving the region of plastic deformation during the CBT process. The volume of material in which the flow stress is greatest is limited to a moving line where the rollers contact the sheet and superimpose bending stress on the applied tensile load. Hence the condition of a large volume of material experiencing stress greater than the material flow stress, leading to strain localization during ST, is avoided. However, the magnitude of the contribution of this phenomenon to the overall increase in elongation is unclear. In the current set of experiments, an elongation to fracture (ETF) of 4.56x and 3.7x higher than ST was achieved by fine-tuning CBT forming parameters for Q&P 1180 and TBF 1180, respectively. A comparison of maximum local strains near the final point of fracture in ST and CBT sheets via digital image correlation revealed that avoidance of localization of plastic strain during CBT accounts for less than half of the increased elongation in the CBT specimens for two steels containing different amounts of retained austenite (RA). Geometrically necessary dislocation evolution is monitored using high-resolution EBSD (HREBSD) for both strain paths, indicating a lower hardening rate in the CBT samples in the bulk of the sheet, potentially relating to the cyclical nature of the stress in the outer layers of the sheet. Interestingly, the GND evolution in the center of the sheet, which does not experience the same amplitude of cyclic stress, follows the ST behavior more closely than the sheet edges. This appears to contribute to a precipitous drop in residual ductility for the specimens that are pulled in ST after partial CBT processing. The rate of transformation of RA is also tracked in the steels, with a significantly lower rate of transformation during CBT, compared to ST. This suggests that a slower transformation rate achieved under CBT also contributed to higher strain-to-failure levels.more » « less
-
Daehn G., Cao J. (Ed.)Controlling the microstructure of components is of interest to achieve optimal final part properties, i.e., materials by design. The manufacturing process itself can affect a material’s characteristics by changing the microstructure. For example, past research has shown that austenite to martensite phase transformation in stainless steel occurs during deformation. Temperature is known to have a significant influence on this phenomenon. In this paper, the effect of temperature on the austenitic to martensite phase transformation in SS 316L under uniaxial tension is investigated. Both a cooling system and a heat exchanger were employed in a uniaxial tension experimental setup to control the temperature. Tensile specimens were strained to fracture at four temperatures of −15, 0, 10, and 20 °C. Digital imaging correlation (DIC) and a thermal imaging camera were used for tests at 0 °C and above to capture strain and temperature data, respectively. Strain and temperature data could not be obtained at −15 °C due to the DIC paint flaking during testing. X-ray diffraction was used to measure the volume fraction of martensite in both the as-received and the tensile-tested materials.more » « less
-
Uniaxial tension is a universal material characterization experiment. However, studies have shown that increased formability can be achieved with simultaneous bending and unbending of the material. This so-called continuous bending under tension process is an example of bending stress superposition to a uniaxial tension process. In this research, experiments are conducted on stainless steel 304 to investigate the effects of bending stress superposition on the austenite to martensite phase transformation. Two vortex tubes are mounted to the carriage of the machine and used to decrease the temperature in a localized region of the specimen to evaluate two temperature conditions. The in-situ strain and temperature fields are captured using 3D digital image correlation and infrared cameras. The deformation induced α′ -martensite volume fraction is measured at regular intervals along the deformed gauge length using a Feritscope. The number of cycles that the rollers traverse the gauge length, corresponding to the strain level, is also varied to create five conditions. The deformed specimens revealed heterogeneous martensite transformation along the gauge length due to the non-uniform temperature fields observed for each test condition. Decreasing the temperature and increasing the number of cycles led to the highest amount of phase transformation for this bending-tension superposed process. These results provide insight on how stress superposition can be applied to vary the phase transformation in more complex manufacturing processes, such as incremental forming, which combines bending, tension, and shear deformation.more » « less
-
Abstract The automotive industry relies heavily on sheet metal forming processes for many components. Material data solely from uniaxial testing is insufficient to fully define the material behavior of the complex plastic deformation during numerical simulations of the forming processes. In-plane biaxial testing using a cruciform type specimen is a more comprehensive representation than the traditional uniaxial testing alone. Wide ranging biaxial stress states can be imposed by applying different loading conditions on each cruciform axis. However, this can create a challenge to achieve desired deformation paths due to the non-linear relationship between the control parameter, e.g., displacement, and the output of interest, e.g., strain path. In this paper, an interpolation method to develop the displacement control that produces a linear strain path with a desired strain ratio is revisited and expanded upon from the authors’ previous work [1,2]. In the first iteration, linear biaxial displacements were applied to the specimen and the corresponding strain paths were obtained from the numerical simulations. The non-linear strain paths, due to geometry effects of the specimen, were used to reverse engineer a new displacement path that results in a linear strain path. Interpolation is revisited to show increased success with a second iteration. Analysis of the simulation results shows that linear strain paths of a given model can be determined and improved by successive iterations of interpolating the strain data from adjacent deformation paths.more » « less
An official website of the United States government
