More Like this

1. HIGH TEMPERATURE CHARACTERIZATION OF FIBER BRAGG GRATING SENSORS EMBEDDED INTO METALLIC STRUCTURES THROUGH ULTRASONIC ADDITIVE MANUFACTURING

   Schomer, J.J. ; Dapino, M.J. ( September 2018 , Proceedings of the ASME 2017 Conference on Smart Materials, Adaptive Structures and Intelligent Systems)

   Embedded fiber Bragg grating (FBG) sensors are attractive for in-situ structural monitoring, especially in fiber reinforced composites. Their implementation in metallic structures is hindered by the thermal limit of the protective coating, typically a polymer material. The purpose of this study is to demonstrate the embedding of FBG sensors into metals with the ultimate objective of using FBG sensors for structural health monitoring of metallic structures. To that end, ultrasonic additive manufacturing (UAM) is utilized. UAM is a solid-state manufacturing process based on ultrasonic metal welding that allows for layered addition of metallic foils without melting. Embedding FBGs through UAM is shown to result in total cross-sectional encapsulation of the sensors within the metal matrix, which encourages uniform strain transfer. Since the UAM process takes place at essentially room temperature, the industry standard acrylate protective coating can be used rather than requiring a new coating applied to the FBGs prior to embedment. Measurements presented in this paper show that UAM-embedded FBG sensors accurately track strain at temperatures higher than 400 C. The data reveals the conditions under which detrimental wavelength hopping takes place due to non-uniformity of the load transferred to the FBG. Further, optical cross-sectioning of the test specimens shows inhibition of the thermal degradation of the protective coating. It is hypothesized that the lack of an atmosphere around the fully-encapsulated FBGs makes it possible to operate the sensors at temperatures well above what has been possible until now. Embedded FBGs were shown to retain their coatings when subjected to a thermal loading that would result in over 50 percent degradation (by volume and mass) in atmospherically exposed fiber. 

   more » « less
2. Detection of Crack Initiation and Growth Using Fiber Bragg Grating Sensors Embedded into Metal Structures through Ultrasonic Additive Manufacturing

   https://doi.org/10.3390/s19224917  

   Chilelli, Sean K. ; Schomer, John J. ; Dapino, Marcelo J. ( November 2019 , Sensors)

   Structural health monitoring (SHM) is a rapidly growing field focused on detecting damage in complex systems before catastrophic failure occurs. Advanced sensor technologies are necessary to fully harness SHM in applications involving harsh or remote environments, life-critical systems, mass-production vehicles, robotic systems, and others. Fiber Bragg Grating (FBG) sensors are attractive for in-situ health monitoring due to their resistance to electromagnetic noise, ability to be multiplexed, and accurate real-time operation. Ultrasonic additive manufacturing (UAM) has been demonstrated for solid-state fabrication of 3D structures with embedded FBG sensors. In this paper, UAM-embedded FBG sensors are investigated with a focus on SHM applications. FBG sensors embedded in an aluminum matrix 3 mm from the initiation site are shown to resolve a minimum crack length of 0.286 ± 0.033 mm and track crack growth until near failure. Accurate crack detection is also demonstrated from FBGs placed 6 mm and 9 mm from the crack initiation site. Regular acrylate-coated FBG sensors are shown to repeatably work at temperatures up to 300 ∘ C once embedded with the UAM process. 

   more » « less
3. Additive Manufacturing of 3D‐Architected Multifunctional Metal Oxides

   https://doi.org/10.1002/adma.201901345  

   Yee, Daryl W. ; Lifson, Max L. ; Edwards, Bryce W. ; Greer, Julia R. ( June 2019 , Advanced Materials)

   Additive manufacturing (AM) of complex three‐dimensional (3D) metal oxides at the micro‐ and nanoscales has attracted considerable attention in recent years. State‐of‐the‐art techniques that use slurry‐based or organic–inorganic photoresins are often hampered by challenges in resin preparation and synthesis, and/or by the limited resolution of patterned features. A facile process for fabricating 3D‐architected metal oxides via the use of an aqueous metal‐ion‐containing photoresin is presented. The efficacy of this process, which is termed photopolymer complex synthesis, is demonstrated by creating nanoarchitected zinc oxide (ZnO) architectures with feature sizes of 250 nm, by first patterning a zinc‐ion‐containing aqueous photoresin using two‐photon lithography and subsequently calcining them at 500 ºC. Transmission electron microscopy (TEM) analysis reveals their microstructure to be nanocrystalline ZnO with grain sizes of 5.1 ± 1.6 nm. In situ compression experiments conducted in a scanning electron microscope show an emergent electromechanical response: a 200 nm mechanical compression of an architected ZnO structure results in a voltage drop of 0.52 mV. This photopolymer complex synthesis provides a pathway to easily create arbitrarily shaped 3D metal oxides that could enable previously impossible devices and smart materials.

    

   more » « less
4. Multifunctional Graphene–Polymer Nanocomposite Sensors Formed by One-Step In Situ Shear Exfoliation of Graphite

   https://doi.org/10.3390/jcs7080309  

   Ashraf, Ali ; Chang, Elizabeth ; Rahman, Md Ashiqur ; Ghosh, Dipannita ; Islam, Nazmul ; Lynch-Branzoi, Jennifer K. ( August 2023 , Journal of Composites Science)

   Graphene nanocomposites are a promising class of advanced materials for sensing applications; yet, their commercialization is hindered due to impurity incorporation during fabrication and high costs. The aim of this work is to prepare graphene–polysulfone (G−PSU) and graphene–polyvinylidene fluoride (G−PVDF) nanocomposites that perform as multifunctional sensors and are formed using a one-step, in situ exfoliation process whereby graphite is exfoliated into graphene nanoflakes (GNFs) directly within the polymer. This low-cost method creates a nanocomposite while avoiding impurity exposure since the raw materials used in the in situ shear exfoliation process are graphite and polymers. The morphology, structure, thermal properties, and flexural properties were determined for G−PSU and G−PVDF nanocomposites, as well as the electromechanical sensor capability during cyclic flexural loading, temperature sensor testing while heating and cooling, and electrochemical sensor capability to detect dopamine while sensing data wirelessly. G−PSU and G−PVDF nanocomposites show superior mechanical characteristics (gauge factor around 27 and significantly enhanced modulus), thermal characteristics (stability up to 500 °C and 170 °C for G−PSU and G−PVDF, respectively), electrical characteristics (0.1 S/m and 1 S/m conductivity for G−PSU and G−PVDF, respectively), and distinguished resonant peaks for wireless sensing (~212 MHz and ~429 MHz). These uniquely formed G−PMC nanocomposites are promising candidates as strain sensors for structural health monitoring, as temperature sensors for use in automobiles and aerospace applications, and as electrochemical sensors for health care and disease diagnostics.

    

   more » « less
5. Experimental Investigation on Forming Limit Curve at Elevated Temperature Through Dome and Biaxial Test

   https://doi.org/10.1115/IMECE2020-23085  

   Nikhare, Chetan P. ; Teculver, Evan ; Aqlan, Faisal ( November 2020 , Proceedings of the ASME 2020 International Mechanical Engineering Congress and Exposition)

   null (Ed.)

   The characteristics of metal and materials are very important to design any component so that it should not fail in the life of the service. The properties of the materials are also an important consideration while setting the manufacturing parameters which deforms the raw material to give the design shape without providing any defect or fracture. For centuries the commonly used method to characterize the material is the traditional uniaxial tension test. The standard has been created for this test by American Standard for Testing Materials (ASTM) – E8. This specimen is traditionally been used to test the materials and extract the properties needed for designing and manufacturing. It should be noted that the uniaxial tension test uses one axis to test the material i.e., the material is pulled in one direction to extract the properties. The data acquired from this test found enough for manufacturing operations of simple forming where one axis stretching is dominant. Recently a sudden increase in the usage of automotive vehicles results in sudden increases in fuel consumption which results in an increase in air pollution. To cope up with this challenge federal government is implying the stricter environmental regulation to decrease air pollution. To save from the environmental regulation penalty vehicle industry is researching innovation which would reduce vehicle weight and decrease fuel consumption. Thus, the innovation related to light-weighting is not only an option anymore but became a mandatory necessity to decrease fuel consumption. To achieve this target, the industry has been looking at fabricating components from high strength to ultra-high strength steels or lightweight materials. This need is driven by the requirement of 54 miles per gallon by 2025. In addition, the complexity in design increased where multiple individual parts are eliminated. This integrated complex part needs the complex manufacturing forming operation as well as the process like warm or hot forming for maximum formability. The complex forming process will induce the multi-axial stress states in the part, which is found difficult to predict using conventional tools like tension test material characterization. In many pieces of literature limiting dome height and bulge tests were suggested analyzing these multi-axial stress states. However, these tests limit the possibilities of applying multi-axial loading and resulting stress patterns due to contact surfaces. Thus, a test machine called biaxial test is devised which would provide the capability to test the specimen in multi-axial stress states with varying load. In this paper, two processes, limiting dome test and biaxial test were experimented to plot the forming limit curve. The forming limit curve serves the tool for the design of die for manufacturing operation. For experiments, the cruciform test specimens were used in both limiting dome test and biaxial test and tested at elevated temperatures. The forming limit curve from both tests was plotted and compared. In addition, the strain path, forming, and formability was investigated and the difference between the tests was provided. 

   more » « less