skip to main content


Title: Electrochemical Polishing of Extruded and Laser Powder-Bed-Fused Inconel 718
ABSTRACTElectro-chemical polishing (ECP) was utilized to produce sub-micron surface finish on Inconel 718 parts manufactured by Laser Powder-Bed-Fusion (L-PBF) and extrusion methods. The L-PBF parts had very rough surfaces due to semi-welded powder particles, surface defects, and difference layer steps that were generally not found on surfaces of extruded and machined components. This study compared the results of electro-polishing of these differently manufactured parts under the same conditions. Titanium electrode was used with an acid-based electrolyte to polish both the specimens at different combinations of pulsed current density, duty cycle, and polishing time. Digital 3D optical profiler was used to assess the surface finish, while optical and scanning electron microscopy was utilized to observe the microstructure of polished specimens. At optimal condition, the ECP successfully reduced the surface of L-PBF part from 17 µm to 0.25 µm; further polishing did not improve the surface finish due to different removal rates of micro-leveled pores, cracks, nonconductive phases, and carbide particles in 3D-printed Inconel 718. The microstructure of extruded materials was uniform and free of processing defects, therefore can be polished consistently to 0.20 µm. Over-polishing of extruded material could improve its surface finish, but not for the L-PBF material due to defects and the surrounding micro-strain.  more » « less
Award ID(s):
1711917
NSF-PAR ID:
10323991
Author(s) / Creator(s):
; ; ;
Date Published:
Journal Name:
International Journal of Engineering Materials and Manufacture
Volume:
6
Issue:
4
ISSN:
0128-1852
Page Range / eLocation ID:
284 to 298
Format(s):
Medium: X
Sponsoring Org:
National Science Foundation
More Like this
  1. The ability of Additive Manufacturing (AM) processes to ensure delivery of high quality metal-based components is somewhat limited by insufficient inspection capabilities. The inspection of AM parts presents particular challenges due to the design flexibility that the fabrication method affords. The nondestructive evaluation (NDE) methods employed need to be selected based on the material properties, type of possible defects, and geometry of the parts. Electromagnetic method, in particular Eddy Current (EC), is proposed for the inspections. This evaluation of EC inspection considers surface and near-surface defects in a stainless steel (SS) 17 4 PH additively manufactured sample and a SS 17 4 PH annealed plates manufactured traditionally (reference sample). The surfaces of the samples were polished using 1 micron polishing Alumina grit to achieve a mirror like surface finish. 1.02 mm (0.04”), 0.508 mm (0.02”) and 0.203 mm (0.008”) deep Electronic Discharge Machining (EDM) notches were created on the polished surface of the samples. Lift off and defect responses for both additive and reference samples were obtained using a VMEC-1 commercial instrument and a 500 kHz absolute probe. The inspection results as well as conductivity assessments for the AM sample in terms of the impedance plane signature were compared to response of similar features in the reference sample. Direct measurement of electromagnetic properties of the AM samples is required for precise inspection of the parts. Results show that quantitative comparison of the AM and traditional materials help for the development of EC technology for inspection of additively manufactured metal parts. 
    more » « less
  2. null (Ed.)
    Abstract An experimental study was conducted to study the effects of geometric size and surface treatment on the fatigue life of fused filament fabrication (FFF) manufactured acrylonitrile butadiene styrene (ABS) parts. Moore rotating-beam fatigue tests were conducted with four different levels of loadings to obtain the S–N curves. Two different sizes (control size and large size) and three different surface treatment methods (as-printed, acetone-treated, and sandpaper polished) were studied. The larger specimens had significantly decreased fatigue life because of a larger volume, and hence a greater probability of defects for crack initiation and propagation, as compared with the control specimen. The acetone-treated specimen had a smooth surface. Its fatigue life, however, decreased significantly because the acetone treatment caused internal damage that weakened the specimen and was reported for the first time. The sandpaper polished specimen also had a smooth surface, but its effect on the fatigue life was insignificant because the extruded filament direction on the specimen surface was parallel to the loading direction. The present results lead to a better understanding of the effects of geometric size and surface treatment on the fatigue performance of FFF specimens. The study also provides important insights for the design of part size and surface treatment of three-dimensional (3D) printed plastic components for fatigue loading end-use applications. 
    more » « less
  3. Abstract

    The present work utilizes Orientation Imaging Microscopy and Finite Element Modelling to analyse microstructure evolution in grains near defects during plane strain indentation of direct metal laser sintered Inconel 718. Defects are inevitably produced during printing of metals and they degrade the mechanical behaviour of parent components. Understanding microstructure evolution of grains present near defects can help create better predictive models of mechanical behaviour of components resulting from additive manufacturing. In this work, an ex-situ study of microstructure evolution during plane strain indentation of DMLS Inconel 718 specimens is performed. Regions that lie near volumetric porosity defects were studied. Grain Orientation Spread was utilized as a metric to quantify intra-granular deformation. It was seen that microstructure evolution of grains near defects is enhanced due to strain concentrations whereby they exhibit larger orientation spread after plastic deformation. Finite Element Analysis was used to simulate the plane strain indentation test on the specimen in which, porosity defects and roughness textures similar to those seen in the as-received specimen were programmed using the python scripting interface of Abaqus. Results from finite element analysis were compared with insights from microstructure analysis to describe evolution of microstructure during deformation near defects.

     
    more » « less
  4. Abstract Laser powder bed fusion (L-PBF) additive manufacturing (AM) is an effective method of fabricating nickel–titanium (NiTi) shape memory alloys (SMAs) with complex geometries, unique functional properties, and tailored material compositions. However, with the increase of Ni content in NiTi powder feedstock, the ability to produce high-quality parts is notably reduced due to the emergence of macroscopic defects such as warpage, elevated edge/corner, delamination, and excessive surface roughness. This study explores the printability of a nickel-rich NiTi powder, where printability refers to the ability to fabricate macro-defect-free parts. Specifically, single track experiments were first conducted to select key processing parameter settings for cubic specimen fabrication. Machine learning classification techniques were implemented to predict the printable space. The reliability of the predicted printable space was verified by further cubic specimens fabrication, and the relationship between processing parameters and potential macro-defect modes was investigated. Results indicated that laser power was critical to the printability of high Ni content NiTi powder. In the low laser power setting (P < 100 W), the printable space was relatively wider with delamination as the main macro-defect mode. In the sub-high laser power condition (100 W ≤ P ≤ 200 W), the printable space was narrowed to a low hatch spacing region with macro-defects of warpage, elevated edge/corner, and delamination happened at different scanning speeds and hatch spacing combinations. The rough surface defect emerged when further increasing the laser power (P > 200 W), leading to a further narrowed printable space. 
    more » « less
  5. The quality of powder processed for manufacturing can be certified by hundreds of different variables. Assessing the impact of all these different metrics on the performance of additively manufactured engineered products is an invaluable, but time intensive specification process. In this work, a comprehensive, generalizable, data-driven framework was implemented to select the optimal powder processing and microstructure variables that are required to predict the target property variables. The framework was demonstrated on a high-dimensional dataset collected from selective laser melted, additively manufactured, Inconel 718. One hundred and twenty-nine powder quality variables including particle morphology, rheology, chemical composition, and build composition, were assessed for their impact on eight microstructural features and sixteen mechanical properties. The importance of each powder and microstructure variable was determined by using statistical analysis and machine learning models. The trained models predicted target mechanical properties with an R2 value of 0.9 or higher. The results indicate that the desired mechanical properties can be achieved by controlling only a few critical powder properties and without the need for collecting microstructure data. This framework significantly reduces the time and cost of qualifying source materials for production by determining an optimal subset of experiments needed to predict that a given source material will lead to a desired outcome. This general framework can be easily applied to other material systems. 
    more » « less