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The newly developed FeMnAlNiTi shape memory alloy (SMA) holds significant promise due to its desirable properties including ease of processing, room temperature superelasticity, a wide superelastic window of operation, and high transformation stress levels. In this study, we report single crystals with tensile axis near h123i exhibiting transformation strains of 9% with a high trans- formation stress of 700 MPa. The functional performance revealed excellent recovery of 98% of the applied strain in an incremental strain test for each of the 40 applied cycles. Concomitantly, the total residual strain increased after each cycle. Accumulation of residual martensite is observed possibly due to pinning of austenite/martensite (A/M) interface. Subsequently, under structural fatigue loading with a constant strain amplitude of 1%, the recoverable strains saturate around 1.15% in local residual martensite domains. Intermittent enhancement of recoverable strains is observed due to transformation triggered in previously untransformed domains. Eventually, fatigue failure occur- red after 2046 cycles and the dominant mechanism for failure was microcrack initiation and coalescence along the A/M interface. Thus, it is concluded that interfacial dislo- cations, which play a crucial role in the superelastic (SE) functionality, invariably affect the structural fatigue per- formance by acting as the weakest link in the microstructure.
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Mechanical fatigue in microtubules
Mechanical failure of biological nanostructures due to sustained force application has been studied in great detail. In contrast, fatigue failure arising from repeated application of subcritical stresses has received little attention despite its prominent role in engineering and potentially biology. Here, paclitaxel-stabilized microtubules are up to 256 times bent into sinusoidal shapes of varying wavelength and the frequency of breaking events are observed. These experiments allow the calculation of fatigue life parameters for microtubules. Repeated buckling due to 12.5% compression–equal to the compression level experienced by microtubules in contracting cardiomyocytes – results in failure after in average 5 million cycles, whereas at 20.0% compression failure occurs after in average one thousand cycles. The fatigue strength (Basquin) exponent B is estimated as − 0.054±0.009.
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- Award ID(s):
- 2230116
- PAR ID:
- 10646548
- Publisher / Repository:
- Nature Publishing Group
- Date Published:
- Journal Name:
- Scientific Reports
- Volume:
- 14
- Issue:
- 1
- ISSN:
- 2045-2322
- Page Range / eLocation ID:
- 26336
- Subject(s) / Keyword(s):
- Fatigue failure, Fatigue strength exponent, Microtubule, Tubulin, Mechanobiology
- Format(s):
- Medium: X
- Sponsoring Org:
- National Science Foundation
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- Free Publicly Accessible Full Text
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Accepted Manuscript1.0
- Journal Article:
- https://doi.org/10.1038/s41598-024-76409-7
